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40 results about "Dication" patented technology

A dication is any cation, of general formula X²⁺, formed by the removal of two electrons from a neutral species. Diatomic dications corresponding to stable neutral species (e.g. H2+ 2 formed by removal of two electrons from H₂) often decay quickly into two singly charged particles (H⁺), due to the loss of electrons in bonding molecular orbitals. Energy levels of diatomic dications can be studied with good resolution by measuring the yield of pairs of zero-kinetic-energy electrons from double photoionization of a molecule as a function of the photoionizing wavelength (threshold photoelectrons coincidence spectroscopy – TPEsCO). The He2+ 2 dication is kinetically stable.

Dication asphalt emulsifier containing ethoxy as well as preparation method and application of dication asphalt emulsifier

The invention discloses a dication asphalt emulsifier containing ethoxy as well as a preparation method and application of the dication asphalt emulsifier. The emulsifier has a structural formula shown in the specification. The preparation method of the emulsifier comprises the following steps: dissolving fatty alcohol-polyoxyethylene ether into an organic solvent, adding a catalyst, adding sodium hydroxide after the fatty alcohol-polyoxyethylene ether is dissolved, and stirring to dissolve sodium hydroxide; adding an intermediate B after 30 minutes; performing magnetic stirring at 50-70DEG C to react for 6-12 hours; cooling to the room temperature, and then performing reduced pressure distillation, washing and carrying out suction filtration; performing vacuum drying at 40 DEG C to obtain an intermediate C; dissolving the intermediate C into the organic solvent, adding a catalyst, adding sodium hydroxide after the intermediate C is dissolved, and adding epoxy propyl-trimethyl ammonium chloride to react for 6-12 hours; and performing washing, suction filtration and drying to obtain a product. The asphalt emulsifier disclosed by the invention is low in raw material price and production cost, the preparation method is simple in process and low in reaction temperature, and the temperature needed by synthetic reaction is 40-70 DEG C. In the structural formula shown in the specification, n is equal to 12, 14, 16 or 18, and m is equal to 3, 5, 7, 9, 15, 20 or 25.
Owner:HEBEI UNIV OF TECH

Dication asphalt emulsifier and preparation method thereof

The invention discloses a dication asphalt emulsifier. The molecular structure of the dication asphalt emulsifier is shown in the description, wherein when x is equal to 1, y is equal to 1 and i is equal to 0; when x is equal to 2, y is equal to 0, z is equal to 1 or 0, and i plus z is equal to 1. The dication asphalt emulsifier is prepared from the following raw material in molar ratio: 1 mol of N-Hydrogenated tallow-1, 3-diaminopropane, 6.00-13.00 mol of alcohols solvent, 1.02-3.05 mol of methyl acrylate, and 2.02-2.10 mol of sodium chloroacetate. The alcohols solvent adopts ethyl alcohol, methyl alcohol or isopropyl alcohol. The synthetic raw material of the dication asphalt emulsifier is easy to get, the production cost is low, the technology is simple, and high-temperature reaction is not required. Different types of asphalt can be emulsified, the prepared asphalt emulsifier is exquisite and uniform, the storage stability is good, dication emulsified asphalt can be prepared, and the dication asphalt emulsifier is applied to spreading of road penetrated oil layers or bonding oil as well as slurry surfacing and micro-surfacing parts, and has the characteristics of a medium breaking asphalt emulsifier and a slow breaking asphalt emulsifier.
Owner:SHANDONG UNIV

Method for extracting and separating phenolic compound in oil-phenol mixture by using quaternary ammonium dication liquid

The invention provides a method for extracting and separating a phenolic compound in an oil-phenol mixture by using quaternary ammonium dication liquid. The method comprises the following steps: adding a given amount of quaternary ammonium dication liquid extracting agent into an oil-phenol mixture, stirring at given temperature, enabling the phenolic compound in the oil-phenol mixture to form a deep-eutectic solvent with the quaternary ammonium dication liquid extracting agent, and separating from an oil phase, thus separating the phenolic compound in the oil-phenol mixture, wherein by virtue of a liquid separation method, the deep-eutectic solvent is separated, then a back-extractant is added into the deep-eutectic solvent, the quaternary ammonium dication liquid extracting agent is precipitated in a solid form, and the quaternary ammonium dication liquid extracting agent is obtained by virtue of filtering and separating can be repeatedly used; the phenolic compound in the back-extractant is recovered in a distilling method, and the back-extractant is repeatedly used. The quaternary ammonium dication liquid extracting agent used in the method is environmentally friendly, good in heat stability, not soluble in the oil phase, high in extraction rate and reusable.
Owner:BEIJING UNIV OF CHEM TECH
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