Method for preparing methyl methacrylate from reactive amide salt
A technology of methyl methacrylate and crude methyl methacrylate, applied in the direction of amide preparation, carboxylate separation/purification, carboxylate preparation, etc., to achieve the effect of simple process, high purity and easy control
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[0035] Embodiment 1: as figure 1 Shown, this prepares the method for methyl methacrylate by reaction amide salt, comprises the following steps:
[0036] (1) the amide salt adopts a plurality of esterification reactors connected in series with gas phase and liquid phase lined PTFE pipelines to carry out multiple esterification reactions successively, and gather the gas phase materials after multiple esterification reactions;
[0037] S11 The reaction amide salt from the amide reactor enters the first esterification reactor 1 by gravity and is hydrolyzed into methacrylic acid, and methanol is passed into the first esterification reactor 1, and in the first esterification reactor 1 The temperature of the gas phase is controlled by cascade adjustment of the water phase from the extractor in the regulator FIC and the gas phase temperature TIC of the first esterification reactor 1, and the low boilers containing methanol and MMA from the rectification process are controlled by the r...
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