Method for adsorbing radioactive iodine
A technology of radioactive iodine and adsorbent, applied in the direction of radioactive purification, separation methods, chemical instruments and methods, etc., can solve problems such as explosion and fire, and achieve the effect of maintaining fire resistance
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Embodiment 1
[0033] H 3 BO 3 (4g) and C 3 N 6 h 6 (4 g) was added to 200 mL of distilled water. The mixture was stirred to 85 °C for complete dissolution and stirring was continued for 6 hours, then cooled to ambient temperature to produce a white precipitate. After filtration, the precipitate was washed with cold deionized water and dried overnight to obtain the precursor. Transfer the precursor to a corundum tube. Porous boron nitride was subsequently produced by a multi-step pyrolysis process: the precursor was preheated at 550 °C for 2 h, then heated at 2 °C min -1 The rate was slowly heated to 1100°C and kept for 2 hours, and finally calcined at 1200°C for 4 hours. All reactions were carried out under the protection of argon.
Embodiment 2
[0035] H 3 BO 3 (4g) and C 3 N 6 h 6 (4 g) was added to 200 mL of distilled water. The mixture was stirred to 85 °C for complete dissolution and stirring was continued for 6 hours, then cooled to ambient temperature to produce a white precipitate. After filtration, the precipitate was washed with cold deionized water and dried overnight to obtain the precursor. Transfer the precursor to a corundum tube. Porous boron nitride was subsequently produced by a multi-step pyrolysis process: the precursor was preheated at 550 °C for 2 h, then heated at 2 °C min -1 The rate was slowly heated to 1100°C and kept for 2 hours, and finally calcined at 1250°C for 4 hours. All reactions were carried out under the protection of argon.
Embodiment 3
[0037] H 3 BO 3 (4g) and C 3 N 6 h 6 (4 g) was added to 200 mL of distilled water. The mixture was stirred to 85 °C for complete dissolution and stirring was continued for 6 hours, then cooled to ambient temperature to produce a white precipitate. After filtration, the precipitate was washed with cold deionized water and dried overnight to obtain the precursor. Transfer the precursor to a corundum tube. Porous boron nitride was subsequently produced by a multi-step pyrolysis process: the precursor was preheated at 550 °C for 2 h, then heated at 2 °C min -1 The rate was slowly heated to 1100°C and kept for 2 hours, and finally calcined at 1300°C for 4 hours. All reactions were carried out under the protection of argon.
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