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Method for evaluating anaerobic digestion performance of lignocellulosic feedstocks by pretreatment intensity

A technology of lignocellulose and anaerobic digestion, which is applied in the field of organic solid waste treatment and disposal - anaerobic digestion, can solve the problems of difficult implementation and heavy performance evaluation workload, and reduce the experimental workload and mathematical model Calculation and fitting, the effect of saving anaerobic digestion time

Active Publication Date: 2020-09-04
BEIJING UNIV OF CHEM TECH
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] Aiming at the problem that the performance evaluation of anaerobic digestion of lignocellulosic raw materials after different hydrothermal pretreatments is heavy and difficult to realize, the present invention is proposed
[0006] Aiming at the problem that the performance evaluation of anaerobic digestion of lignocellulosic raw materials after different hydrothermal pretreatments is heavy and difficult to realize, the present invention is proposed

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  • Method for evaluating anaerobic digestion performance of lignocellulosic feedstocks by pretreatment intensity
  • Method for evaluating anaerobic digestion performance of lignocellulosic feedstocks by pretreatment intensity
  • Method for evaluating anaerobic digestion performance of lignocellulosic feedstocks by pretreatment intensity

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Embodiment 1

[0064] (1) Hydrothermal pretreatment

[0065] Weigh 20g of corn stalks and calculate with raw material TS. The pretreatment experiment is divided into two groups, one group is hydrothermally pretreated alone, and the other group is added with 2% of the dry weight of corn stalks at the same time. 3 ·H 2 O; add ammonia hydrothermal pretreatment group to add 2% ammonia water of dry weight of corn stalks, and then adjust its moisture content to 80%; add tap water to the single hydrothermal group, and adjust its moisture content to 80%. Add raw materials and water into a glass container, stir evenly with a glass rod, and then place in a hydrothermal reactor for heating pretreatment. The pretreatment conditions set for corn straw pretreatment are: at 50°C, the pretreatment time is 1d, 2d, 3d; at 70°C, the pretreatment time is 1d, 2d; The pretreatment time is 5min, 10min, 20min, 30min, 150℃, the pretreatment time is 5min, 10min, 20min and 200℃, the pretreatment time is 5min, 10min....

Embodiment 2

[0084] (1) Hydrothermal pretreatment

[0085] Weigh 20g of rice husk and calculate it based on raw material TS. The pretreatment experiment is divided into two groups, one group is hydrothermally pretreated alone, and the other group is added with 2% NH of corn stalk dry weight at the same time. 3 ·H 2 O; add ammonia hydrothermal pretreatment group to add 2% of the dry weight of rice husk ammonia water, and then adjust its moisture content to 80%; add tap water to the separate hydrothermal group, and adjust its moisture content to 80%. Add raw materials and water into a glass container, stir evenly with a glass rod, and then place in a hydrothermal reactor for heating pretreatment. The pretreatment conditions set for rice husk pretreatment are: at 50°C, the pretreatment time is 1d, 3d, at 70°C, the pretreatment time is 1d, 3d, at 90°C, the pretreatment time is 2h, 4h, and at 100°C The pretreatment time is 5min, 30min, 150°C, 5min, 10min, and 200°C, 5min, 10min. Three groups...

Embodiment 3

[0105] (1) Hydrothermal pretreatment

[0106] Weigh 20g of cow dung and calculate it based on raw material TS. The pretreatment experiment is hydrothermal pretreatment alone. Tap water is added to the cow dung to adjust its moisture content to 80%. Add raw materials and water into a glass container, stir evenly with a glass rod, and then place in a hydrothermal reactor for heating pretreatment. The pretreatment conditions set for cow dung pretreatment are: pretreatment time at 50°C is 1d, 3d, pretreatment time at 70°C is 1d, 3d, pretreatment time at 90°C is 2h, 4h, pretreatment at 100°C The pretreatment time is 5min, 30min, 150°C, 5min, 10min, and 200°C, 5min, 10min. Three groups of parallels were set under each pretreatment condition.

[0107] After the pretreatment, use water cooling and air cooling to cool down. After the cooling is completed, the cow dung is taken out, and the properties of pH, reducing sugar, VFAs, etc. after pretreatment and whether there are toxic and...

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Abstract

The invention discloses a method for evaluating anaerobic digestion performance of a lignocellulose raw material by means of the pretreatment strength, and belongs to the field of anaerobic digestionof organic solid wastes. The method comprises the following steps: adding a reagent into the lignocellulose raw material, carrying out hydrothermal pretreatment at certain temperature under certain time condition, and measuring the pH value of the pretreated raw material; calculating the hydrothermal pretreatment intensity under different conditions; inoculating sludge, adding water to a constantvolume, and carrying out anaerobic fermentation; and fitting the hydrothermal intensity with the methane yield to evaluate the methane potential process. The method has the following advantages that (1) the provided hydrothermal intensity evaluation method reduces complex mathematical model calculation and fitting; (2) the experimental workload and the required time can be greatly reduced, and theanaerobic digestion time can be saved (30-60d); and (3) the operation is simple, the price is low, and the time required for COD test as well as the waste liquid treatment cost can be reduced; and (4) operation is simple and rapid, energy is saved, and the environment is protected.

Description

technical field [0001] The invention belongs to the field of anaerobic digestion for organic solid waste treatment and disposal, and specifically relates to a method for judging the methane production performance of anaerobic digestion of lignocellulosic raw materials after hydrothermal pretreatment by using pretreatment intensity. Background technique [0002] Lignocellulosic biomass is a huge carbon resource on the earth and is considered to be the most promising substitute for petroleum. However, the complex structure of lignocellulosic raw materials hinders the contact between cellulase and lignocellulose, making lignocellulose difficult to degrade. Therefore, in order to improve the methane-producing ability of lignocellulosic raw materials, many scholars have developed various pretreatment methods to destroy the spatial structure of lignocellulose, making it easier to contact with microorganisms and enzymes, so as to improve the gas-producing performance. Since anaero...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N25/00G01N30/02
CPCG01N25/00G01N30/02Y02E50/30
Inventor 袁海荣王喜彤李秀金
Owner BEIJING UNIV OF CHEM TECH