Novel high-purity acetylene purification production system and technological process thereof

A production system and acetylene generator technology, which is applied in the purification/separation of hydrocarbons, chemical change purification/separation, organic chemistry, etc., can solve the problem of purification purity not meeting the requirements of customers, high cost, and achieve impurity removal. The effect of enhancing the effect, increasing the contact time, and increasing the contact area

Pending Publication Date: 2020-02-28
金昌隆博气体有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the country has not issued a national standard for high-purity acetylene, but the quality requirements of the customer's receipt, the purity must reach more than 99%, and the silver nitrate test paper cannot change color
[0004] At present, the production process of dissolved acetylene mainly consists of four units of acetylene generation, purificati...

Method used

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  • Novel high-purity acetylene purification production system and technological process thereof
  • Novel high-purity acetylene purification production system and technological process thereof
  • Novel high-purity acetylene purification production system and technological process thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] Such as Figure 1 to Figure 2As shown, a new type of high-purity acetylene purification production system includes calcium carbide slag sedimentation tank, acetylene generator, acetylene gas cabinet, safety water seal, purification tower, purification tower water tank, neutralization tower, neutralization tower water tank, Gas-water separator, low-temperature dryer, compressor, high-pressure oil-water separator drying box and acetylene filling system, the height of the packing layer of the purification tower is 7-11m, and the purification tower includes the first purification tower and the second purification tower , the second purification tower is connected to the neutralization tower.

[0038] The specific steps for the purification and production of acetylene gas by using the above-mentioned new high-purity acetylene purification production system are as follows:

[0039] (1) The process flow of acetylene gas: put a certain amount of water in the acetylene generato...

Embodiment 2

[0044] Such as Figure 1 to Figure 2 As shown, in order to make the present invention have a better purification effect in the purification tower 5, this embodiment has made further improvements on the basis of Embodiment 1, specifically: each of the purification towers 5 is provided with 6 spray heads 503, a Pall ring is added at the spray head 503 in the purification tower 5.

Embodiment 3

[0046] Such as Figure 1 to Figure 2 Shown in order to make the consumption cost of sodium hypochlorite solution of the present invention, present embodiment has done further improvement on the basis of embodiment 2, specifically: described purification tower 5 water tanks are two, and described two purification towers 5 all connect A water tank and a circulating water pump 601 connected with the water tank are provided.

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Abstract

The invention discloses a novel high-purity acetylene purification production system and a technological process thereof, belonging to the technical field of acetylene production. The high-purity acetylene purification production system provided by the invention is high in purification degree and capable of saving cost. The system comprises a carbide slag settling pond, an acetylene generator, anacetylene gasometer, a safety water seal, a purifying tower, a purifying tower water tank, a neutralizing tower, a neutralizing tower water tank, a gas-water separator, a low-pressure dryer, a compressor, a high-pressure oil-water separator drying box and an acetylene filling system which are connected in sequence, wherein the height of a packing layer of the purification tower is 7-11m, the purification tower comprises a first purification tower and a second purification tower, and the second purification tower is connected with the neutralizing tower. The high-purity acetylene purification production system designed by the invention is high in acetylene purification purity which can reach 99% or above, and is reduced in the use cost of sodium hypochlorite.

Description

technical field [0001] The invention relates to the technical field of acetylene production, and in particular to a novel high-purity acetylene purification production system and its process flow, which are used for the purification production of high-purity acetylene. Background technique [0002] Acetylene, also called calcium carbide gas, is a colorless, slightly toxic and flammable gas with weak anesthesia and preventing cell oxidation at normal temperature and pressure. The explosion limit in air is 2.5% to 80%. Pure acetylene has no smell, but because the calcium sulfide and phosphide contained a small amount of calcium sulfide and phosphide in the calcium carbide raw material for the production of acetylene, solid industrial acetylene contains phosphine, hydrogen sulfide and other impurities and has an unpleasant garlic smell. It cannot be liquefied under normal pressure, hardly soluble in water, easily soluble in petroleum ether, ethanol, benzene and other organic s...

Claims

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Application Information

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IPC IPC(8): B01D53/75B01D53/78B01D53/52B01D53/48B01D53/46C07C7/00C07C7/148C07C11/24
CPCB01D53/46B01D53/485B01D53/52B01D53/75B01D53/78B01D2251/108B01D2251/304B01D2251/604B01D2257/30B01D2257/55B01D2257/553C07C7/005C07C7/148C07C11/24
Inventor 尹爱华尹建华王坤杰关文杰李成生何静霞张云龙
Owner 金昌隆博气体有限责任公司
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