Melanin-nano selenium and its preparation method
A technology of melanin and nano-selenium, applied in the field of chemistry, can solve the problems of high cost, harsh reaction conditions, toxic reducing agent and template agent, etc., and achieve the effects of low cost, mild reaction conditions and wide sources.
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[0036] The present invention will be specifically introduced below in conjunction with the accompanying drawings and specific embodiments.
[0037] 1. Preparation of melanin-nano selenium
[0038] Weigh 5.55mg of selenium dioxide, dissolve it with distilled water and make it up to 10mL to obtain a selenium dioxide stock solution with a concentration of 0.555mg / mL.
[0039] Weighed 3.0 mg of black sesame melanin, dissolved it with disodium hydrogen phosphate-citric acid buffer solution with pH=8.0, and adjusted the volume to 10 mL to obtain a melanin stock solution with a concentration of 0.3 mg / mL.
[0040] Measure 5mL selenium dioxide stock solution and 9mL melanin stock solution (mass ratio of selenium dioxide to melanin is 1:1), dilute with a small amount of distilled water respectively, then mix and adjust the volume to 45mL, stir to make the solution fully mixed, and then use Dilute hydrochloric acid and sodium hydroxide adjust the pH of the solution to make the pH of th...
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