Check patentability & draft patents in minutes with Patsnap Eureka AI!

Melanin-nano selenium and its preparation method

A technology of melanin and nano-selenium, applied in the field of chemistry, can solve the problems of high cost, harsh reaction conditions, toxic reducing agent and template agent, etc., and achieve the effects of low cost, mild reaction conditions and wide sources.

Active Publication Date: 2022-02-22
ZHONGBEI UNIV
View PDF0 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] For the preparation of nano-selenium, the chemical reduction method is mostly used at present, but this method has the disadvantages of harsh reaction conditions, high cost, toxic reducing agent and template agent, etc.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Melanin-nano selenium and its preparation method
  • Melanin-nano selenium and its preparation method
  • Melanin-nano selenium and its preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0036] The present invention will be specifically introduced below in conjunction with the accompanying drawings and specific embodiments.

[0037] 1. Preparation of melanin-nano selenium

[0038] Weigh 5.55mg of selenium dioxide, dissolve it with distilled water and make it up to 10mL to obtain a selenium dioxide stock solution with a concentration of 0.555mg / mL.

[0039] Weighed 3.0 mg of black sesame melanin, dissolved it with disodium hydrogen phosphate-citric acid buffer solution with pH=8.0, and adjusted the volume to 10 mL to obtain a melanin stock solution with a concentration of 0.3 mg / mL.

[0040] Measure 5mL selenium dioxide stock solution and 9mL melanin stock solution (mass ratio of selenium dioxide to melanin is 1:1), dilute with a small amount of distilled water respectively, then mix and adjust the volume to 45mL, stir to make the solution fully mixed, and then use Dilute hydrochloric acid and sodium hydroxide adjust the pH of the solution to make the pH of th...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a melanin-nano-selenium and a preparation method thereof, wherein the preparation method uses melanin as a reducing agent and a template for nano-selenium structure synthesis, and uses melanin to reduce a selenium dioxide solution, specifically comprising the following steps: preparing selenium dioxide Stock solution and melanin stock solution, then dilute the stock solution, mix and adjust the pH to 8.5, react in a dark, normal pressure environment at a constant temperature of 40°C, and stir in a constant speed water bath for 5 hours to obtain a sample, then filter the sample and collect the filtrate The melanin-nano-selenium solution is obtained, and finally the obtained melanin-nano-selenium solution is vacuum freeze-dried to obtain melanin-nano-selenium particles. The benefits of the present invention are: mild reaction conditions, easy implementation; wide source of melanin, low cost, excellent physical and chemical properties such as biodegradability, redox and metal chelation, non-toxic, and is an ideal reducing agent and templating agents.

Description

technical field [0001] The invention relates to nano-selenium and a preparation method thereof, in particular to melanin-nano-selenium and a preparation method thereof, and belongs to the field of chemical technology. Background technique [0002] Selenium is the active center of various enzymes in organisms, can participate in the body's antioxidant and energy metabolism, and is an essential substance to maintain the normal vitality of the body. A large number of studies have shown that nano-selenium has better bioavailability and lower toxicity than inorganic selenium and traditional organic selenium supplements, which makes nano-selenium a new focus in the research field and has a good role in the development of selenium supplementation products. application prospects. [0003] For the preparation of nano-selenium, the chemical reduction method is mostly used at present, but this method has disadvantages such as harsh reaction conditions, high cost, and toxic reducing ag...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C01B19/02B82Y30/00B82Y40/00
CPCC01B19/02B82Y30/00B82Y40/00
Inventor 赵英虎高莉任燕玲郭丽晓王芳王海宾史楠郭建峰
Owner ZHONGBEI UNIV
Features
  • R&D
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More