A method for starting an activated coke dry adsorption purification device

A purification device and active coke technology, applied in chemical instruments and methods, separation methods, dispersed particle separation, etc., can solve the problems of long start-up process and inconvenience of timely commissioning, shorten start-up time, reduce adsorption activity, and shorten start-up time Effect

Active Publication Date: 2022-04-05
SINOPEC ENG +1
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

When the existing active coke dry purification device is started for the first time, the amount of flue gas introduced initially is only 40-50% of the design load, and the temperature of the flue gas is controlled not to exceed 120°C. After the activated coke adsorption tower is operated for 7-8 days, the adsorption activity will be corresponding After the reduction, gradually increase the flue gas volume to the normal design load. The whole start-up process is relatively long, usually 7-10 days, which brings some inconvenience to the timely commissioning of the device.

Method used

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  • A method for starting an activated coke dry adsorption purification device
  • A method for starting an activated coke dry adsorption purification device

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Embodiment

[0077] Use figure 1The reactive coke method is used to adsorb the purification device, and the starting method includes:

[0078] Step (1): Before the active focal absorbent tower is introduced into the flue gas start, open the valve J, open the butterfly valve L and butterfly valve M, turn off the butterfly valve G and butterfly valve K, slowly start the net flue gas boost fan E, introduce normal temperature air 11, Gradually establish air in active focal absorbent tie B --net flue gas boost fan E - 气 Cooler D --- activity focusing between Tight Tie B, then gradually increases net flue gas boost fan E The speed continues to introduce normal temperature air 11. When the speed of the net flue gas boost fan E is close to the design speed, and the active focal absorbent tower B pressure tends to stabilize, the valve J is closed, and the air is closed and closed, and the flue gas cooler D is opened, and there are many stable operation. Fresh-active focus was performed in 12 to 24 hour...

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Abstract

The invention relates to a start-up method of an active coke dry adsorption purification device. The method comprises the following steps: (1) introducing air into an active coke adsorption tower equipped with fresh active coke to passivate the fresh active coke; (2) nitrogen enters the activated coke adsorption tower to replace at least part of the air; (3) introduces the flue gas to be purified into the activated coke adsorption tower, the initial introduction of the flue gas to be purified does not exceed 80% of the device design load, gradually Increase the introduction of flue gas to be purified until it reaches 100% of the design load of the device, and the activated coke dry adsorption purification device operates normally. The start-up method of the present invention adopts air circulation to passivate the active coke before introducing the flue gas to reduce its adsorption activity and avoid overheating of the active coke bed when the flue gas is introduced, and the air passivation process of the active coke can be independent of the The upstream system is carried out in advance, which shortens the start-up time of the device and ensures the safe and stable operation of the active coke adsorption tower.

Description

Technical field [0001] The present invention relates to the field of active ocuroscopic flue gas desulfurization process, and in particular, to a method of starting a chemical adsorption purification apparatus. Background technique [0002] The activated coke method has begun industrial applications in the 1980s, with high desulfurization efficiency, reactive water, no wastewater waste, no equipment corrosion problems. With the increasing environmental requirements, this technology has attracted more and more attention, and it is widely used. Applying active coke method purification techniques to catalytic cracking devices, which can effectively remove SO in regenerated flue gas 2 / SO 3 At the same time x , Particulate matter and VOCS, etc. also have a synergistic removal effect, combined with the upstream SCR and downstream bag dust collector, and the entire purification system can purify the smoke to meet the standard requirements. [0003] The active coke adsite is mainly bas...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D53/04
CPCB01D53/04
Inventor 黄孟旗张喆周桂娟郝少博魏志强
Owner SINOPEC ENG
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