Antistatic regenerated polyester composite air filtering material and preparation method thereof
An air filter material and recycled polyester technology, which is applied in the manufacture of conductive/antistatic filaments, filtration separation, membrane filters, etc., can solve the problems of small porosity, high cost, and poor strength
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[0021] The invention provides a preparation method of an antistatic regenerated polyester composite air filter material, comprising the following steps:
[0022] (1) The graphene powder and the polyamide master batch are initially mixed and twin-screw blended, extruded and granulated in turn to obtain the graphene / polyamide blended master batch;
[0023] (2) twin-screw blending and extruding granulation of the graphene / polyamide blending masterbatch and regenerated polyester masterbatch to obtain graphene / polyamide / regenerated polyester blending masterbatch;
[0024] (3) melt-spinning the graphene / polyamide / regenerated polyester blend masterbatch to obtain mixed fibers;
[0025] (4) heat-treating a part of the mixed fiber to obtain bulked yarn short fiber; weaving the yarn into plain weave fabric after spinning the other part;
[0026] The bulky yarn staple fiber is air-laid to obtain a bulky yarn staple fiber web; the bulky yarn staple fiber web is fixed on the surface of a ...
Embodiment 1
[0036] The graphene powder (zinc oxide doped graphene) with a particle size of 2 μm and a polyamide 6 master batch (particle size of 2 mm) are placed in an internal mixer according to a mass ratio of 1:4, and the mixing temperature is 230°C for 10min; then put the initial mixture into a twin-screw extruder for blending and granulation, the blending temperature is 235°C, and the time is 15min to obtain a graphene / polyamide blend masterbatch with a particle size of 2mm ;
[0037] The graphene / polyamide blend masterbatch and bottle flakes recycled polyester masterbatch (particle size 1mm) were put into a twin-screw extruder in a mass ratio of 1:1 for blending and granulation. The blending temperature was 240°C, and the time For 20min, graphene / polyamide / recycled polyester blend masterbatch was obtained, and the particle size was 2mm;
[0038] The graphene / polyamide / regenerated polyester blend masterbatch was melt-spun through a twin-screw spinning machine, the spinning temperatu...
Embodiment 2
[0043] The graphene powder (porous graphene) with a particle size of 3 μm is placed in an internal mixer according to the mass ratio of 1:3 and polyamide 66 (with a particle size of 5 mm), and the mixing temperature is 270 ° C and the time is 5min; then put the initial mixture into the twin-screw extruder for blending and granulation, the blending temperature is 270°C, and the time is 10min to obtain graphene / polyamide blend masterbatch, with a particle size of 5mm;
[0044] The graphene / polyamide blend masterbatch and bottle flake recycled polyester masterbatch (particle size 3mm) were put into a twin-screw extruder at a mass ratio of 1:1 for blending and granulation. The blending temperature was 230°C, and the time For 15min, graphene / polyamide / recycled polyester blend masterbatch was obtained, and the particle size was 5mm;
[0045] The graphene / polyamide / regenerated polyester blend masterbatch was melt-spun through a twin-screw spinning machine, the spinning temperature wa...
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Abstract
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