Fixed bed reactor for methane oxidative coupling reaction and method for preparing ethylene by methane oxidative coupling

A fixed bed reactor, oxidative coupling reaction technology, applied in chemical instruments and methods, condensation hydrocarbon production with dehydrogenated hydrocarbons, organic chemistry, etc., can solve problems such as poor industrial implementation

Active Publication Date: 2020-10-09
CHINA PETROLEUM & CHEM CORP +1
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0008] In view of the deficiencies in the above-mentioned prior art, the purpose of the present invention is to solve the problem of poor industrial implementation in the prior art, and to provide an industrially implementable, small reaction temperature rise, and heat

Method used

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  • Fixed bed reactor for methane oxidative coupling reaction and method for preparing ethylene by methane oxidative coupling
  • Fixed bed reactor for methane oxidative coupling reaction and method for preparing ethylene by methane oxidative coupling
  • Fixed bed reactor for methane oxidative coupling reaction and method for preparing ethylene by methane oxidative coupling

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Embodiment 1

[0031] Such as figure 1 A fixed-bed reactor for methane oxidative coupling reaction shown, the reactor includes a reactor shell (cylindrical body) and an oxygen distributor arranged in the reactor shell, a catalyst bed, 12 U-shaped heat extraction tube bundle, high-pressure steam superheating section; the oxygen distributor is arranged on the upper part of the catalyst bed, and the high-pressure steam superheating section is arranged on the lower part of the catalyst bed;

[0032] Such as figure 2 and image 3 As shown, the catalyst bed is divided into upper and lower layers, the upper layer is an insulating layer, and the lower layer is an approximately isothermal layer. The U-shaped heat extraction tube bundle is arranged in the approximate isothermal layer, and 4 U-shaped heat extraction tube bundles are used for high pressure saturation. Steam, 4 U-shaped heat extraction tube bundles are used to superheat high-pressure saturated steam. Valves are installed on the 4 U-sh...

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Abstract

The invention belongs to the field of preparation of ethylene by oxidative coupling of methane, and particularly relates to a fixed bed reactor for oxidative coupling reaction of methane and a methodfor preparing ethylene by oxidative coupling of methane. The reactor comprises a reactor shell, and comprises a catalyst bed layer, a plurality of U-shaped heat removal pipe bundles and a high-pressure steam overheating section which are arranged in the reactor shell, wherein the high-pressure steam overheating section is arranged at the lower part of the catalyst bed layer; the catalyst bed layeris divided into an upper layer and a lower layer, the upper layer is a heat-insulating layer, and the lower layer is an approximately isothermal layer; the multiple U-shaped heat removal pipe bundlesare arranged in the approximate isothermal layer, one part of the pipe bundles are used for generating high-pressure saturated steam, and the other part of the pipe bundles are used for overheating the high-pressure saturated steam. The invention provides an ideal reactor and a control scheme which can be implemented industrially, are small in reaction temperature rise, good in heating effect, high in ethylene selectivity and convenient and adjustable in system for the reaction for preparing ethylene through oxidative coupling of methane, and promote industrialization of preparing ethylene through oxidative coupling of methane.

Description

technical field [0001] The invention belongs to the field of ethylene production through oxidative coupling of methane, and more specifically relates to a fixed-bed reactor for oxidative coupling reaction of methane and a method for producing ethylene through oxidative coupling of methane. Background technique [0002] Ethylene is one of the largest chemical products in the world. The ethylene industry is the core of the petrochemical industry. Ethylene products account for more than 75% of petrochemical products and occupy an important position in the national economy. The world has taken ethylene production as one of the important symbols to measure the development level of a country's petrochemical industry. [0003] With the sharp fluctuation of international crude oil prices and technological progress, in order to change the situation that ethylene production raw materials are overly dependent on petroleum resources, the production of ethylene raw materials has changed....

Claims

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Application Information

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IPC IPC(8): B01J8/02B01J8/00C07C2/84C07C11/04
CPCB01J8/001B01J8/008B01J8/0285C07C2/84B01J2208/00132B01J2208/00495C07C11/04Y02P20/52
Inventor 聂毅强王振维丁利伟孙丽丽刘罡盛在行赵百仁
Owner CHINA PETROLEUM & CHEM CORP
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