Composite phase-change material, preparation method thereof and phase-change cold storage device
A technology of composite phase change materials and mixtures, applied in heat exchange materials, chemical instruments and methods, heat storage equipment, etc., can solve problems such as poor flame retardancy and thermal stability, and achieve improved thermal stability and low production costs. , the effect of simple components
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[0031] In one embodiment of the present application, the above preparation method includes: mixing the materials comprising molten paraffin and expanded graphite and performing first stirring to obtain the first mixture; mixing the materials comprising molten hydrotalcite and calcium stearate mixing and performing a second stirring to obtain a second mixture; mixing the first mixture and the second mixture and performing a third stirring to obtain a composite phase change material.
[0032] When the composite phase change material includes paraffin, hydrotalcite, expanded graphite and calcium stearate, since the viscosity of molten paraffin and hydrotalcite is relatively large, the paraffin, hydrotalcite, expanded graphite and calcium stearate are directly mixed, It is easy to cause uneven mixing, thereby affecting the flame retardancy, thermal stability and other properties of the final composite phase change material. The above preparation method first stirs the expanded gra...
Embodiment 1
[0041] Heat 760g of paraffin to 40-45°C, and stop heating after it is in a completely molten state to obtain molten paraffin. Heat 255g of hydrotalcite to 75-80°C, and stop heating after it is in a completely molten state to obtain molten hydrotalcite.
[0042] The molten paraffin and the molten hydrotalcite were mixed and stirred to obtain 1000 g of a composite phase change material, wherein the stirring speed was 1000 r / min, and the stirring time was 2 hours. In terms of mass percentage, the paraffin content in the composite phase change material is 75%, the phase change temperature is 20-25°C, and the hydrotalcite content is 25%.
Embodiment 2
[0044] The difference between embodiment 2 and embodiment 1 is that
[0045] The rotational speed of the first stirring is 500r / min, and the stirring time of the first stirring is 4h, and finally a composite phase change material is obtained. In terms of mass percentage, the paraffin content in the composite phase change material is 75%, and the phase change temperature is 20-25°C. , The hydrotalcite content is 25%.
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