Recapture agent, preparation method and method for treating trivalent chromium in electroplating wastewater
A technology for electroplating wastewater and trivalent chromium, which is applied in the fields of metallurgical wastewater treatment, water/sewage treatment, chemical instruments and methods, etc. It can solve the problems of poor pertinence, poor electroplating wastewater treatment effect, and inability to meet standards in one-time treatment. , to achieve the effect of cost reduction, good treatment effect and strong treatment pertinence
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Embodiment 1
[0039] A 500g small airtight reactor with temperature control is used to prepare a recapture agent for trivalent chromium ions in electroplating wastewater:
[0040] 1.1 Raw materials, the amount of raw materials is shown in Table 1 below:
[0041] Table 1 Embodiment 1 raw material list:
[0042]
[0043] 1.2 Preparation method, comprising the following steps:
[0044] (1) Alcohol water is mixed with mass concentration and is the alcohol solution of 40%; Hydroxide water is configured with mass concentration and is the hydroxide solution of 25%;
[0045] (2) Add hexamethylenediamine and the alcohol solution prepared in step (1) into the reaction vessel at a room temperature of 25°C, and mix and stir for 18 minutes to obtain a mixed solution A;
[0046] (3) The temperature of the mixed solution A in the reaction vessel was lowered to 5°C, and carbon disulfide was added dropwise to the reaction vessel at a constant speed under stirring, and the dropwise addition was complete...
Embodiment 2
[0051] A 500g small airtight reactor with temperature control is used to prepare a recapture agent for trivalent chromium ions in electroplating wastewater:
[0052] 2.1 Raw materials, the amount of raw materials is shown in Table 2 below:
[0053] Table 2 Embodiment 2 raw material table:
[0054]
[0055] 2.2 Preparation method, comprising the following steps:
[0056] (1) Alcohol water is mixed with mass concentration and is the alcohol solution of 60%; Hydroxide water is configured with mass concentration and is the hydroxide solution of 15%;
[0057](2) Add hexamethylenediamine and the alcohol solution prepared in step (1) into the reaction vessel at a room temperature of 25°C, and mix and stir for 15 minutes to obtain a mixed solution A;
[0058] (3) The temperature of the mixed solution A in the reaction vessel was lowered to 10°C, and carbon disulfide was added dropwise to the reaction vessel at a constant speed under stirring, and the dropwise addition was complet...
Embodiment 3
[0063] A 500g small airtight reactor with temperature control is used to prepare a recapture agent for trivalent chromium ions in electroplating wastewater:
[0064] 3.1 Raw materials, the amount of raw materials is shown in Table 3 below:
[0065] Table 3 Embodiment 3 raw material table:
[0066]
[0067] 3.2 Preparation method, comprising the following steps:
[0068] (1) Alcohol water is mixed with mass concentration and is the alcohol solution of 20%; Hydroxide water is configured with mass concentration and is the hydroxide solution of 40%;
[0069] (2) At room temperature, add hexamethylenediamine and the alcohol solution prepared in step (1) into the reaction vessel, and mix and stir for 18 minutes to obtain mixed solution A;
[0070] (3) Lower the temperature of the mixed solution A in the reaction vessel to 7°C, and add carbon disulfide dropwise to the reaction vessel at a constant speed under stirring; after the dropwise addition, keep the temperature at 7°C and...
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