Electroplating method based simple super-hydrophobic tube inner surface preparation device

A super-hydrophobic surface and a technology for preparing devices, which are applied in electrolytic components, electrolytic processes, cells, etc., can solve problems such as limited operation, low surface uniformity, and expensive equipment

Inactive Publication Date: 2020-10-30
DALIAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to solve the problems of limited operation of the inner surface, expensive equipment cost, complicated process flow and low surface uniformity in the existing technology of the superhydrophobic surface inside the circular tube, and proposes a simple superhydrophobic inner surface of the tube based on the electroplating method Preparation device, electroplating a layer of uniform and fine coating on the inner wall of the pipeline to achieve a stable hydrophobic structure, which solves the problem of difficulty in achieving superhydrophobicity on the inner wall of the pipeline

Method used

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  • Electroplating method based simple super-hydrophobic tube inner surface preparation device

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Embodiment 1

[0024] 1. Pre-treatment of pipe fittings: take a copper pipe with a length of 500mm and an inner diameter of 10mm as the pipe fitting to be plated, perform surface polishing, stain removal, and degreasing treatment, then activate for 30S, clean it with deionized water, and dry it to obtain the treated pipe. Workpiece; Activation Solution Components: HCL with a volume fraction of 10%.

[0025] 2. Installation of pipe fittings: first install the pipe fitting 5 to be plated on the base 2, slowly move the electroplating anode 4 vertically down to the groove of the base 2, and then screw in the screw rod 9 to complete the sealing of the device.

[0026] 3. Electroplating: nickel rods are used as the electroplating anode 4, the workpiece after pretreatment is the cathode 5, the radial distance between the two poles is 4mm, electroplating is carried out in the basic electroplating solution, the distance between the electrodes is 2mm, the specific parameters of electrodeposition: pump ...

Embodiment 2

[0028] 1. Pre-treatment of pipe fittings: use Q235 steel pipes with a length of 500mm and an inner diameter of 10mm as the pipe fittings to be plated, perform surface polishing, stain removal, and degreasing treatment, then activate for one minute, clean them with deionized water, and dry them to obtain processed Workpiece; Activation solution composition: 0.07mol / L of H 2 SO 4 .

[0029] 2. Installation of pipe fittings: first install the pipe fitting 5 to be plated on the base 2, slowly move the electroplating anode 4 vertically down to the groove of the base 2, and then screw in the screw rod 9 to complete the sealing of the device.

[0030] 3. Electroplating: the copper tube is used as the electroplating anode 4, the workpiece after pretreatment is the cathode 5, and the radial distance between the two poles is 2mm. Electroplating is carried out in the basic electroplating solution, and the distance between the electrodes is 4mm. The specific parameters of electrodepositi...

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Abstract

The invention discloses an electroplating method based simple super-hydrophobic tube inner surface preparation device. The electroplating method based simple super-hydrophobic tube inner surface preparation device comprises a tube fitting and an electroplating anode which are coaxially arranged between a base and a top plate, wherein a lead screw passes through the top plate and the base for enclosing the electroplating anode and the tube fitting into a sealed reaction cavity; a conductive copper sheet is mounted on the upper surface, at the top end of the tube fitting, of the electroplating anode; the upper side surface of the conductive copper sheet is connected to a guide wire; the guide wire is accessed into a power supply through a top plate through hole; the top plate and the tube fitting are provided with openings, and are accessed into a circulating pipeline; a peristaltic pump drives a solution in a plating solution slot to enter the tube fitting to react, and then flow back into the plating solution slot to accomplish a cycle; and an ultrasonic transducer is mounted at the lower end of the base, and is coaxial with the tube fitting. The electroplating method based simplesuper-hydrophobic tube inner surface preparation device solves the problem that in-tube super-hydrophobic surface preparation is difficult, has the advantages of being high in cost performance, conveniently and quickly replacing the tube fitting, being strong in sealing property, adopting ultrasonic cavitation effect to reduce retention of gas bubbles in an electroplating process, and acceleratessurface reaction, so that uniformity of a hydrophobic surface structure is improved, and the purpose of controlling surface topography can be achieved by programing specified current output.

Description

technical field [0001] The invention belongs to the technical field of material surface modification, in particular to a simple super-hydrophobic tube inner surface preparation device based on an electroplating method. Background technique [0002] Surface wettability is an important property of the surface of solid materials. Changing the wettability of the solid surface to hydrophilic or hydrophobic can effectively improve some shortcomings of the material and expand the application range of the material. The solid surface with superhydrophobic properties is almost in a non-wetting state after contact with water droplets, and this state plays an important role in anti-freezing, microfluidics, pipeline drag reduction, anti-corrosion and self-cleaning. After further research, it was found that , the micro-nano rough structure on the surface is the main reason for achieving superhydrophobic properties. [0003] Although there are many methods for preparing superhydrophobic s...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C25D17/00C25D5/20C25D5/02C25D7/04C25D21/04C25D21/18C25D21/12C25D5/34C25D3/12
CPCC25D17/00C25D5/20C25D5/028C25D7/04C25D21/04C25D21/18C25D21/12C25D5/34C25D3/12
Inventor 姜洪鹏白敏丽吕继组高林松邢志远
Owner DALIAN UNIV OF TECH
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