Water-resistant environment-friendly fiber filtering material and preparation method thereof
A filter material and nanofiber technology, applied in the field of water-resistant environmental protection fiber filter material and its preparation, can solve the problems of poor water resistance, loss of fiber structure, etc. Effect
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Embodiment 1
[0035] 1. A method for preparing water-resistant polyvinyl alcohol nanofibers, comprising the following steps:
[0036] Weigh 9g of polyvinyl alcohol (1799, degree of alcoholysis 98% (mol / mol)) and mix with 120mL of distilled water, heat to 85°C with stirring, and keep warm for 1.5h to obtain a polyvinyl alcohol fiber solution; Add 0.826g(-)-epigallocatechin and 29.7g L-2-amino-3-methylbutyric acid, heat to 105°C, stir for 1.2h, let stand and cool to obtain surface-modified polyvinyl alcohol The fiber solution is precipitated with acetone, and the product is filtered, and the filtrate is repeatedly washed with distilled water for 3 times, dried and ground. Take the modified polyvinyl alcohol, add water at 92°C and stir to dissolve, prepare 150g 8wt% modified polyvinyl alcohol fiber aqueous solution as the electrospinning liquid, according to the ambient temperature of 25°C, humidity of 28%, receiving distance of 18cm, spinning voltage Electrospinning under the condition of 26...
Embodiment 2
[0040] No (-)-epigallocatechin was added to the surface modification of the polyvinyl alcohol fibers, and the remaining parts were exactly the same as in Example 1.
Embodiment 3
[0042]When carrying out surface modification to polyvinyl alcohol fibers, no L-2-amino-3-methylbutyric acid was added, and the rest were exactly the same as in Example 1.
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