High-porosity micrometer porous NiO/Ni material/high-porosity nanometer porous NiO/Ni material and production method and special equipment thereof
A high-porosity, nano-porous technology, applied in the field of high-porosity micro/nano-porous NiO/Ni materials and their preparation, can solve the problems of uncontrollable shape and pore morphology of Ni-Al sintered blanks, difficult to prepare, etc. Effects of reduced charge transfer resistance and interfacial impedance, short reaction time, and abundant pores
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0041] Embodiment 1: according to the atomic ratio of nickel powder and aluminum powder, it is 1:1 to take raw materials, such as getting 11.8g nickel powder and 5.4g aluminum powder respectively, it is poured into the ball mill tank and carried out 4h uniform mixing, with Anhydrous ethanol is used as the ball milling medium; the mixed solution after ball milling is poured into a beaker, and put into a drying oven to dry for 24 hours; about 0.3g of the mixed powder is weighed, poured into a specific mold for pressing, and the obtained product is about d10mm×1mm The cylindrical green body is put into a vacuum tube furnace for heating, first heated to 480°C for 3 hours at a heating rate of 10°C / min, and then continued to heat up to 700°C for 10 minutes to obtain a micron with high porosity and a complete shape. Porous NiAl material. Configure 20wt.% NaOH corrosion solution, then cool to room temperature with the furnace, put the cleaned and dried sintered body into a test tube w...
Embodiment 2
[0046] Embodiment 2: according to the atomic ratio of nickel powder and aluminum powder, it is 1:1 to take raw materials, such as getting 11.8g nickel powder and 5.4g aluminum powder respectively, it is poured into the ball mill tank and carried out 4h uniform mixing, with Anhydrous ethanol is used as the ball milling medium; the mixed solution after ball milling is poured into a beaker, and put into a drying oven to dry for 24 hours; about 0.3g of the mixed powder is weighed, poured into a specific mold for pressing, and the obtained product is about d10mm×1mm The cylindrical green body is put into a vacuum tube furnace for heating, first heated to 480°C for 3 hours at a heating rate of 10°C / min, and then continued to heat up to 700°C for 10 minutes to obtain a micron with high porosity and a complete shape. Porous NiAl material. Prepare 20wt.% NaOH corrosive solution, then cool to room temperature with the furnace, put the cleaned and dried sintered body into a test tube wit...
Embodiment 3
[0048] Embodiment 3: according to the atomic ratio of nickel powder and aluminum powder, be 1:1 to take raw material, for example get 11.8g nickel powder and 5.4g aluminum powder respectively, it is poured into the ball mill jar and carry out 4h uniform mixing, with Anhydrous ethanol is used as the ball milling medium; the mixed solution after ball milling is poured into a beaker, and put into a drying oven to dry for 24 hours; about 0.3g of the mixed powder is weighed, poured into a specific mold for pressing, and the obtained product is about d10mm×1mm The cylindrical green body is put into a vacuum tube furnace for heating, first heated to 480°C for 3 hours at a heating rate of 10°C / min, and then continued to heat up to 700°C for 10 minutes to obtain a micron with high porosity and a complete shape. Porous NiAl material. Prepare 20wt.% NaOH corrosion solution, then cool to room temperature with the furnace, put the cleaned and dried sintered body into a test tube filled wit...
PUM
| Property | Measurement | Unit |
|---|---|---|
| size | aaaaa | aaaaa |
| size | aaaaa | aaaaa |
| porosity | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More