A kind of sound-absorbing material and its preparation method and application
A technology of sound-absorbing material and mixed liquid, applied in the field of sound-absorbing material, can solve the problems of no adhesion of structure, poor sound-absorbing effect, low flame retardant performance, etc., and achieve the effect of improving quality, convenient construction and improving flame retardancy
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Embodiment 1
[0071] The sound-absorbing material of the present embodiment is prepared from the following material:
[0072] Microporous ceramics: Microporous ceramics of different particle sizes are used and mixed in different proportions (as shown in Table 1).
[0073]Modified epoxy resin: 1.84kg, titanium dioxide: 3.22kg, inorganic silicon: 2.88kg, flame retardant: 2.54kg, zirconia: 3kg, water-based silica sol: 3.2kg, ethanol: 3.32kg.
[0074] Curing agent: 2.4kg.
[0075] i) put the flame retardant 2.54kg and the inorganic silicon 2.88kg into the reaction tank in turn, heat it to 175 °C, stir for 20 minutes, cool to 26 °C, to obtain the first mixture;
[0076] ii) to step i) to the first mixture obtained by adding titanium dioxide 3.22kg, aqueous silica sol 3.2kg, zirconia 3kg, modified epoxy resin 1.84kg stirred evenly, to give the 2nd mixture;
[0077] iii) The second mixture obtained in step ii) was ground twice by a stick pin sand mill, and then 3.32 kg of ethanol was added and stirred...
Embodiment 2
[0084] Example 2: Screening test for preparing a mixture of sound-absorbing material C
[0085] Using the weight percentage of the raw material shown in Table 2, 7 mixtures C are configured by the following method:
[0086] i) the flame retardant and inorganic silicon are successively put into the reaction tank, heated to 175 ° C, stirred for 20 minutes, cooled to 26 ° C, to obtain the first mixture;
[0087] ii) to step i) the resulting mixture of titanium dioxide, aqueous silica sol, zirconium dioxide, modified epoxy resin stirred evenly, to give the second mixture;
[0088] iii) the second mixture obtained in step ii) was ground twice by a rod pin sand mill, and then ethanol was added and stirred for 20 minutes to give the mixture C.
[0089] The viscosity, adhesion and impact strength of the obtained mixture C sample 1, 2, 3, 4, 5, 6 and 7 are determined, and the determination method is as follows: The determination of dynamic viscosity is carried out in accordance with GB / T97...
Embodiment 3
[0102] Example 3: The effect of temperature on the final sound-absorbing material
[0103] i) Put the flame retardant and the inorganic silicon into the reaction tank in turn and heat it to T 31 , stir for 20 minutes, cool to 26 ° C, to give the first mixture;
[0104] ii) to step i) the resulting mixture of titanium dioxide, aqueous silica sol, zirconium dioxide, modified epoxy resin stirred evenly, to give the second mixture;
[0105]iii) the second mixture obtained in step ii) was ground twice by a rod pin sand mill, and then ethanol was added and stirred for 20 minutes to give the mixture C.
[0106] The different Ts shown by Table 5 below 31 The preparation of the mixture C, according to the method described in Example 1, wherein the use of microporous ceramic particles with a particle size of 4mm and 3mm, a weight ratio of 7:3 to prepare the corresponding sound-absorbing plates, and then determine the sound-absorbing effect of each sound-absorbing plate.
[0107] Table 5:
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