Preparation methods of spheroidic tungsten trioxide sensitive material and sulfur dioxide gas sensor and evaluation method
A gas sensor, tungsten trioxide technology, used in material resistance, material analysis, material analysis using radiation diffraction, etc., can solve problems such as endangering the personal safety of operation and maintenance personnel, reducing equipment insulation performance, discharge and overheating, etc., to achieve excellent The effect of gas-sensing properties
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[0055]The preparation method of the spherical tungsten trioxide sensitive material provided by the present invention will now be described. The preparation method of the spherical tungsten trioxide sensitive material includes:
[0056]Step 1: Put tungsten hexachloride into a container, add absolute ethanol, and stir to form a solution;
[0057]Step two: adding diammonium hydrogen citrate to the solution and stirring to form a suspension;
[0058]Step 3: Transfer the suspension into an autoclave, heat and react for a certain period of time, and cool naturally to obtain a product precursor;
[0059]Step 4: Collect the product precursors and wash them with deionized water and absolute ethanol;
[0060]Step 5, vacuum drying the washed product precursor;
[0061]The dried product precursor is heated and sintered in a muffle furnace to obtain a spherical tungsten trioxide sensitive material.
[0062]Compared with the prior art, the method for preparing the spherical tungsten trioxide sensitive material provid...
Example Embodiment
[0082]Example 1, a kind of SF based on spherical tungsten trioxide sensitive material6Decomposition product sulfur dioxide gas sensor, at different temperatures (20±1℃~250±2℃) for 100±1μL / L SO2The detection:
[0083]Step one, turn on the precision digital multimeter, programmable DC power supply and computer. Open the software "Fluke" on the computer and set to collect once every 1s. Plug the manufactured sulfur dioxide gas sensor into the test socket, you can immediately see the real-time resistance of the sulfur dioxide gas sensor on the display screen of the precision digital multimeter, and you can see the resistance change curve on the software window. Adjust the output current value of the programmable DC power supply, change the temperature of the sulfur dioxide gas sensor, and stabilize the resistance. Record the resistance R at this timea, Heating current and voltage.
[0084]Step 2: Fill a 1L static gas cylinder with 10±0.1mL SO using a syringe2Gas (the target gas concentration ...
Example Embodiment
[0086]Example 2, SF based on spherical tungsten trioxide sensitive material6Decomposition product sulfur dioxide gas sensor, at different temperatures (20±1℃~250±2℃), for 100μL / L SO2, NH3, Ethanol, methanol, n-butanol and acetone detection:
[0087]Step one, turn on the precision digital multimeter, programmable DC power supply and computer. Open the software "Fluke" on the computer and set to collect once every 1s. Insert the manufactured sulfur dioxide gas sensor into the test socket, you can immediately see the real-time resistance of the sulfur dioxide gas sensor on the display screen of the precision digital multimeter, and the resistance change curve can also be seen on the software window. Adjust the output current value of the programmable DC power supply to make the heating temperature 105±1℃. Record the resistance R at this timea, Heating current and voltage.
[0088]Step 2: Configure 100±1μL / L of SO in a static gas cylinder with a specification of 1L.2, NH3, Ethanol, methanol, ...
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