A kind of ternary metal catalyst and its preparation method and its application in electrolyzing heavy water to prepare deuterium gas
A ternary metal and catalyst technology, applied in electrolysis components, electrolysis process, electrodes, etc., can solve problems such as the difficulty of electrolyzing heavy water, achieve good stability of deuterium analysis, reduce production cost, and evenly distribute
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0033] Concentration of 10 M nitric acid solution pretreatment activated carbon, including the following steps:
[0034] Weigh 1g of activated carbon and add it to 200ml of nitric acid solution with a concentration of 10M, stir at room temperature for 3 h, mix thoroughly, and 2 Heating and stirring treatment at 50°C for 8 hours under the protection of the environment, and then the activated carbon was taken out from the nitric acid solution by centrifugation, and the wet activated carbon was further added to the washing solution, and the activated carbon was washed by centrifugation. The rotational speed of the method is 5000 rpm, the centrifugation time is 5 min, the washing solution is a mixture of water and ethanol, the volume ratio of water and ethanol is 9:1, and the wet activated carbon is washed to pH>6. The washed activated carbon was dried in a vacuum oven at 80° C. for 8 hours to obtain activated carbon A containing oxygen functional groups.
Embodiment 2
[0036] Concentration of 14 M nitric acid solution pretreatment activated carbon, including the following steps:
[0037] Weigh 1g of activated carbon and add it into 500ml of nitric acid solution with a concentration of 14 M, stir at room temperature for 4 h, mix thoroughly, and 2 Heating and stirring treatment at 80°C for 15 h under the protection of the environment, and then the activated carbon was taken out from the nitric acid solution by centrifugation, and the wet activated carbon was further added to the washing solution, and the activated carbon was washed by centrifugation. The centrifugation speed is 10000 rpm, the centrifugation time is 10 min, the washing solution is a mixture of water and ethanol, the volume ratio of water and ethanol is 7:3, and the wet activated carbon is washed to pH>6. The washed activated carbon was dried in a vacuum oven at 80° C. for 8 hours to obtain activated carbon B containing oxygen functional groups.
[0038] The SEM figure and the ...
Embodiment 3
[0040] Concentration of 16 M nitric acid solution pretreatment activated carbon, including the following steps:
[0041] Weigh 1 g of active carbon and add it into 1000 ml of nitric acid solution with a concentration of 16 M, stir at room temperature for 5 h, mix thoroughly, and 2 Heating and stirring treatment at 100°C for 24 h under the protection of the environment, and then the activated carbon was taken out from the nitric acid solution by centrifugation, and the wet activated carbon was further added to the washing solution, and the activated carbon was washed by centrifugation. The centrifugation speed is 15000 rpm, the centrifugation time is 15 min, the washing liquid is a mixture of water and ethanol, the volume ratio of water and ethanol is 1:1, and the wet activated carbon is washed to pH>6. The washed activated carbon was dried in a vacuum oven at 80° C. for 8 hours to obtain activated carbon C containing oxygen functional groups.
PUM
| Property | Measurement | Unit |
|---|---|---|
| particle size (mesh) | aaaaa | aaaaa |
| particle size (mesh) | aaaaa | aaaaa |
| particle size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More