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Graphene hydrogel modified latex and preparation method of graphene modified hydrogel rubber gloves

A graphene hydrogel and modification technology, applied in the field of rubber impregnated gloves, can solve the problems of easy re-stacking of sheets, limiting industrial application, etc.

Inactive Publication Date: 2021-03-12
恒劢安全防护用品(南通)有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, it is easy to re-stack between the sheets, which limits the industrial application

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0055] A graphene hydrogel modified latex formula, comprising the following raw materials in parts by mass: 100 parts of carboxylated nitrile latex, 1 part of KOH, 0.8 parts of sulfur, 2.0 parts of zinc oxide, 1.0 parts of accelerator, 2.0 parts of titanium dioxide, 0.02 parts of dispersant, 20 parts of graphene hydrogel, 0.8 parts of anti-aging agent, 2 parts of black pigment, and 5 parts of cellulose.

[0056] A preparation method for graphene hydrogel multifunctional gloves, comprising the following steps:

[0057] Prepare the latex according to the ratio, control the viscosity at 4000mps, and put it into use after standing for 6 hours;

[0058] Put the HPPE glove core on the hand mold, and preheat the oven at 70°C for 20 minutes;

[0059] Impregnate the coagulant and uniformly coagulate for 70s at room temperature;

[0060] Dip latex, uniform glue 180 at room temperature;

[0061] Sprinkle salt evenly on the glue surface;

[0062] Presulfurization (65°C 60min), soaking...

Embodiment 2

[0065] A graphene hydrogel modified latex formula, comprising the following raw materials in parts by mass: 100 parts of natural latex, 1 part of KOH, 0.8 parts of sulfur, 2.0 parts of zinc oxide, 1.0 parts of accelerator, 2.0 parts of titanium dioxide, and 0.02 parts of dispersant part, 20 parts of graphene hydrogel, 0.8 part of anti-aging agent, 2 parts of black pigment, 5 parts of cellulose.

[0066] A preparation method for graphene hydrogel multifunctional gloves, comprising the following steps:

[0067] Prepare the latex according to the ratio, control the viscosity at 3000mps, and put it into use after standing for 12 hours;

[0068] Put the HPPE glove core on the hand mold, and preheat the oven at 70°C for 30 minutes;

[0069] Impregnate the coagulant and uniformly coagulate for 120s at room temperature;

[0070] Dip latex, homogenize the glue for 240s at room temperature;

[0071] Sprinkle salt evenly on the glue surface;

[0072] Presulfurization (85°C 90min), so...

Embodiment 3

[0075] A graphene hydrogel modified latex formula, comprising the following raw materials in parts by mass: 100 parts of neoprene latex, 1 part of KOH, 0.8 parts of sulfur, 2.0 parts of zinc oxide, 1.0 parts of accelerator, 2.0 parts of titanium dioxide, and dispersant 0.02 parts, 20 parts of graphene hydrogel, 0.8 parts of anti-aging agent, 2 parts of black pigment, 5 parts of cellulose.

[0076] The preparation method of graphene hydrogel multifunctional glove, comprises the following steps:

[0077] Prepare the latex according to the ratio, control the viscosity at 4000mps, put it into use after standing for 6-12 hours;

[0078] Put the HPPE glove core on the hand mold, and preheat the oven at 70°C for 25 minutes;

[0079] Impregnate the coagulant and coagulate evenly for 80s at room temperature;

[0080] Immerse in latex, homogenize the glue for 200s at room temperature;

[0081] Sprinkle salt evenly on the glue surface;

[0082] Presulfurization (80°C 70min), soaking ...

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Abstract

The invention relates to graphene hydrogel modified latex, which comprises the following components in parts by weight: 100 parts of carboxylic butadiene-acrylonitrile rubber, 1-2 parts of potassium hydroxide, 1-1.5 parts of sulfur, 1.5-3 parts of zinc oxide, 0.5-1.2 parts of an accelerant, 0.01-0.03 part of a dispersing agent and 5-50 parts of graphene hydrogel. The preparation method of the graphene modified hydrogel rubber glove comprises the following steps: preparing graphene hydrogel modified latex, controlling the viscosity to be 3000-5000 mps, and performing standing treatment; preheating the glove core; dipping the glove core in a coagulator; dipping the glove core in graphene hydrogel modified latex; uniformly spreading salt on the glue surface for shaping the glove core; and pre-vulcanizing, soaking and washing, and vulcanizing the product. Compared with a traditional glove, the manufactured high-performance protective glove is more resistant to abrasion, tearing, electricity conduction and corrosion.

Description

technical field [0001] The invention belongs to the field of rubber impregnated gloves, in particular to a graphene hydrogel modified latex and a preparation method of graphene modified hydrogel rubber gloves. Background technique [0002] Graphene has many excellent properties, such as large specific surface area, high strength, and high electrical conductivity. Therefore, it is expected to be applied in various fields such as safety protection and electronic materials. However, the easy re-stacking between the sheets limits the industrial application. Graphite oxide is an important derivative of graphene, and graphene-based materials can be obtained through a reduction process. It has gel properties and can form graphene-based hydrogels under certain conditions. Its unique spatial structure can not only prevent sheet restacking, but also can be more conveniently applied to materials. Contents of the invention [0003] In order to solve the above problems, the present...

Claims

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Application Information

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IPC IPC(8): C08L13/02C08L1/02C08L7/02C08L11/02C08K3/22C08K3/06C08K3/04C08K3/16C08K3/00
CPCC08L13/02C08L7/02C08L11/02C08K2003/2296C08K2003/2241C08K2201/001C08L1/02C08K3/22C08K3/06C08K3/042C08K3/16C08K3/00
Inventor 刘网军
Owner 恒劢安全防护用品(南通)有限公司
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