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Method for testing dispersity of SBS modifier in asphalt mixture

A technology of asphalt mixture and testing method, which is applied in the direction of material analysis, measuring device, analyzing material by optical means, etc., can solve the problems of lack of scientificity and rigor, unmeasured actual value, unspecific, etc. Simplification of the environment, good practicality and promotion value, the effect of eliminating interference

Pending Publication Date: 2021-04-16
山东高速路用新材料技术有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, for the dry direct injection process, since the SBS modifier particles are directly mixed into the mixing pot to form a mixture, it is difficult to specifically characterize the dispersion state of the SBS modifier in it. The conventional method is to complete the mixing process. The mixture is tested for various indicators, and the dispersion state of the SBS modifier in the asphalt is indirectly characterized by the test results of the asphalt mixture
However, this method is often highly variable, inaccurate, not specific, and lacks scientific and rigorous
In addition, the traditional visualization-mathematical calculation method (VC method) to measure SBS content / distribution is limited by its measurement principle, and its data collection methods are mostly estimation methods. Even if the results are close to the accurate value through mathematical processing, the actual value However, it cannot be detected by this method
[0004] Therefore, for the dry process, how to ensure that the dry SBS modifier is evenly dispersed in the asphalt mixture in the process of mixing with the aggregate has not been a good analysis method.

Method used

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  • Method for testing dispersity of SBS modifier in asphalt mixture
  • Method for testing dispersity of SBS modifier in asphalt mixture
  • Method for testing dispersity of SBS modifier in asphalt mixture

Examples

Experimental program
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Embodiment 1

[0034] A method for testing the dispersibility of SBS modifier in asphalt, comprising the following steps:

[0035] (1) Disperse sampling is carried out on the modified asphalt mixture to be tested. The sampling position should be clearly differentiated, including the edge, center, bottom layer, and surface layer; add an appropriate amount of carbon tetrachloride (CCl 4 ) to dissolve the sample to obtain a solution for subsequent use;

[0036] (2) Use the calcium fluoride or potassium bromide slide penetration method to carry out infrared testing on the solution of step (1); with the blank slide as the background, the background scan time is 64 times, the sample scan time is 64 times, and the scan speed 7.5KHz, reserved 4000-600cm -1 The data in the interval, the resolution is 4cm -1 ;

[0037] (3) Carry out quantitative analysis to the infrared image of gain, use OPUS software to carry out integral to infrared spectrogram, integrate infrared spectrogram, calculate the area...

Embodiment 2

[0051] In this embodiment, an absorbance-concentration standard curve is drawn with a series of preconfigured concentration gradients of SBS modified asphalt. Both infrared acquisition and data processing use OPUS software, and other data processing software with integral functions can also be used. The area ratio Z after integration i The discrete calculation can use any data processing software.

[0052] Establishment of Absorbance-Dry SBS Dosage Standard Curve

[0053] A certain amount of dry-process SBS modifier particles and No. 70 matrix asphalt were weighed with an analytical balance, dissolved in carbon tetrachloride, and made into a specified concentration of SBS modified asphalt solution. The concentration gradient was set at 4%-6%. 5 groups were set up, and 5 parallel samples were set for each group concentration. When performing infrared measurement, if there is no abnormality in the data of this test, you can move the slide and select a position with a differen...

Embodiment 3

[0058] In this embodiment, the SMA-13 ​​gradation is taken as an example to determine the optimal mixing time of dry SBS under the SMA-13 ​​gradation. Add 7% dry-process SBS modifier to No. 70 asphalt, use basalt coarse aggregate and limestone fine aggregate as stone materials, and set three different mixing times.

[0059] Carry out SBS dispersibility analysis to prepared three groups of mixtures by the method described in the present invention, and Marshall stability test, freeze-thaw splitting experiment, rutting experiment etc., analyze the influence of mixing time on SBS dispersibility, and The effect of the dispersion of dry SBS modifier in asphalt mixture on the macroscopic performance of the specimen.

[0060] 1. Preparation of dry SBS modified asphalt mixture:

[0061] (1) Dry-mix the dry-process SBS modifier and hot aggregate for 60 / 90 / 120s, so that the dry-process SBS modifier is evenly dispersed in the mineral material;

[0062] (2) Add asphalt according to the p...

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Abstract

The invention relates to the technical field of road engineering material detection, in particular to a method for testing dispersity of an SBS modifier in an asphalt mixture. The method for testing the dispersity of the SBS modifier in the asphalt mixture comprises the following steps: (1) dispersing and sampling the asphalt mixture to be tested, dissolving a sample and filtering to obtain a solution; (2) carrying out infrared test on the solution by using a calcium fluoride or potassium bromide slide glass permeation method; (3) carrying out quantitative analysis on the obtained infrared image, carrying out integration on an infrared spectrogram, and calculating areas of two single peaks in respective characteristic peaks of the asphalt and the SBS; (4) recording the ratio of the areas of the two peaks as Z, calculating an average value, analyzing all sampling Zi values, and calculating discreteness; and when the dispersion coefficient is less than 10%, the dispersity meets the requirement. The testing method can characterize the dispersity of the SBS modifier in the asphalt mixture in multiple aspects, facilitates the dispersity evaluation of different SBS modified asphalt mixing and paving processes, and provides a basis for the improvement of a construction process.

Description

technical field [0001] The invention relates to the technical field of road engineering material detection, in particular to a method for testing the dispersibility of SBS modifier in asphalt mixture. Background technique [0002] With the development of modern transportation, traditional asphalt has gradually become difficult to meet the technical requirements of road pavement. Styrene-butadiene-styrene block copolymer (SBS) is an important asphalt modifier, which can effectively improve the high and low temperature performance and rutting resistance of asphalt. At present, the SBS modifier used in industry is mainly wet modification, that is, SBS is ground and mixed with asphalt by means of high-speed shearing to make SBS modified asphalt, and then used in construction. However, the wet process has very obvious limitations, requiring special modification equipment, and the process is complicated; the heating temperature of the asphalt is high, and it is easy to age; the c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/3577G06F17/18
Inventor 白玉铎吴士乾张广威许展飞姜益顺徐大众高国华李传海
Owner 山东高速路用新材料技术有限公司
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