A kind of PVB diaphragm with good weather resistance and preparation method thereof
A performance and weather resistance technology, applied in PVB film with good weather resistance and its preparation field, can solve the problems of general product performance and poor weather resistance
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Embodiment 1
[0029] A kind of good PVB film of weather resistance of the present embodiment comprises the raw material of following weight portion:
[0030] 55 parts of modified grafted PVB resin, 15 parts of graphene emulsion, 10 parts of zeolite-based composite weathering agent, 2 parts of active dispersant, 1 part of dibutyl sebacate toughening agent;
[0031] The preparation method of described modified grafted PVB resin is:
[0032] S1, PVB resin surface treatment: Put the PVB resin into a sodium carbonate solution with a mass fraction of 2% and soak for 10 minutes at a temperature of 45°C, then take it out, dry it, and then irradiate it with cobalt 60-γ rays. Irradiate for 20 minutes, the irradiation power is 150W, and the irradiation is over;
[0033] S2, steam explosion treatment: send PVB resin into the blasting pretreatment liquid, then carry out microwave treatment for 10 minutes, the processing power is 20W, after the treatment is completed, then send it into the steam explosi...
Embodiment 2
[0045] A kind of good PVB film of weather resistance of the present embodiment comprises the raw material of following weight portion:
[0046] 65 parts of modified grafted PVB resin, 25 parts of graphene emulsion, 20 parts of zeolite-based composite weathering agent, 8 parts of active dispersant, 5 parts of dibutyl sebacate toughening agent;
[0047] The preparation method of described modified grafted PVB resin is:
[0048] S1, PVB resin surface treatment: Put the PVB resin into a sodium carbonate solution with a mass fraction of 6% and soak for 20 minutes at a temperature of 55°C, then take it out, dry it, and then irradiate it with cobalt 60-γ rays. Irradiate for 20-30 minutes, the irradiation power is 250W, and the irradiation is over;
[0049] S2, steam explosion treatment: send PVB resin into the blasting pretreatment liquid, then carry out microwave treatment for 20 minutes, the processing power is 50W, after the treatment is completed, then send it into the steam exp...
Embodiment 3
[0059] A kind of good PVB film of weather resistance of the present embodiment comprises the raw material of following weight portion:
[0060] 60 parts of modified grafted PVB resin, 20 parts of graphene emulsion, 15 parts of zeolite-based composite weathering agent, 5 parts of active dispersant, 3 parts of dibutyl sebacate toughening agent;
[0061] The preparation method of described modified grafted PVB resin is:
[0062] S1, PVB resin surface treatment: Put the PVB resin into a sodium carbonate solution with a mass fraction of 4% and soak for 15 minutes at a temperature of 50°C, then take it out, dry it, and then irradiate it with cobalt 60-γ rays. Irradiate for 25 minutes, the irradiation power is 200W, and the irradiation is over;
[0063] S2, steam explosion treatment: send PVB resin into the blasting pretreatment liquid, then carry out microwave treatment for 10-20min, the processing power is 35W, after the treatment is completed, then send it into the steam explosio...
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