Selenium-containing regenerated fiber skin-care antibacterial multifunctional fabric and preparation method thereof
A technology of regenerated fiber, regenerated cellulose, applied in the direction of fiber chemical characteristics, monocomponent cellulose rayon, rayon manufacturing, etc.
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Embodiment 1
[0023] (1) Preparation of selenium-enriched extract: wash Polygonum multiflorum multiflorum to remove surface sediment, mash it, then add 5 times the mass of water, conduct water bath treatment at 80°C for 8 hours, and obtain selenium-enriched extract after filtration.
[0024] (2) Preparation of sodium alginate solution: Soak sodium alginate in water at 35°C for 2 hours to pre-dissolve, then stir for 4 hours at a temperature of 50°C and a rotation speed of 300r / min to prepare sodium alginate with a mass fraction of 10%. solution;
[0025] (3) Preparation of spinning stock solution: under the condition that the temperature is 50°C and the rotating speed is 300r / min, the nano-zinc oxide aqueous dispersion with a mass fraction of 1%, the selenium-enriched extract and the seaweed prepared in step (2) are mixed Sodium acid solution is slowly added in the regenerated cellulose spinning stock solution of cellulose content 8% according to mass ratio, and spinning stock solution solve...
Embodiment 2
[0030] (1) Preparation of selenium-enriched extract: wash Artemisia annua with water to remove surface silt, mash it, then add 5 times the mass of water for 80°C water bath treatment for 8 hours, and obtain selenium-enriched extract after filtration.
[0031] (2) Preparation of sodium alginate solution: Soak sodium alginate in water at 30°C for 3 hours to pre-dissolve, then stir for 5 hours at a temperature of 30°C and a rotation speed of 400r / min to prepare sodium alginate with a mass fraction of 15% solution;
[0032] (3) Preparation of spinning stock solution: under the condition that the temperature is 60°C and the rotating speed is 400r / min, the nano-zinc oxide aqueous dispersion with a mass fraction of 5%, the selenium-enriched extract and the seaweed prepared in step (2) Sodium acid solution is slowly added in the regenerated cellulose spinning stock solution of cellulose content 12% according to mass ratio, and spinning stock solution solvent is sodium hydroxide / thiour...
Embodiment 3
[0037] (1) Preparation of the selenium-enriched extract: wash the honeysuckle vine with water to remove the surface sediment, then mash it, then add 5 times the quality of water and conduct a water bath treatment at 80°C for 8 hours, and obtain the selenium-enriched extract after filtering;
[0038] (2) Preparation of calcium alginate solution: soak calcium alginate in water at 40°C for 2.5 hours to pre-dissolve, then stir for 7 hours at a temperature of 60°C and a rotational speed of 200r / min to prepare alginic acid with a mass fraction of 12%. calcium solution;
[0039] (3) Preparation of spinning stock solution: under the condition that the temperature is 30°C and the rotating speed is 400r / min, the nano-zinc oxide aqueous dispersion with a mass fraction of 3%, the selenium-enriched extract and the seaweed prepared in step (2) Calcium acid solution is slowly added in the regenerated cellulose spinning dope with a cellulose content of 10% according to the mass ratio, and the...
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