A kind of alkyd resin and preparation method thereof
A technology of alkyd resin and basic acid, which is applied in coatings, polyester coatings, etc., can solve the problems of insufficient solid content of coatings, environmental damage, and low gloss, so as to reduce environmental pollution, eliminate treatment costs, and reduce solid content in construction. high effect
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[0047] This example provides a alkyd resin comprising a DinCH by-product 180 kg; propanediol 38kg; trimethylolpropane 240 kg; phthalic anhydride 260kg; ispanyonic acid 160 kg; 1 kg of hypophosphite; phosphite 1kg; xylene 120kg.
[0048] The method of preparing the alkyd resin of the present embodiment is:
[0049] S1, DINCH by-products, propanediol, trimethylolpropane, phthalic anhydride, 160 kg, phosphite triphenyl ester, input reactor, nitrogen gas, flow rate 5m 3 / h, start stirring, heating to the water, heat for 1 h at the effluent temperature, then raised to 230 ° C for 5 h, and 20 kg of xylene is added to 230 ° C to the solid acid value of less than 15 mgKOH / g, the viscosity 25 ° C: Z4 ~ Z6;
[0050] S2, cooling to 120 ° C to 170 ° C, adding residual xylene, stir well.
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