Method for cleaning alkali metal residues and application thereof
An alkali metal and residual technology, applied in the directions of cleaning methods and utensils, chemical instruments and methods, and process efficiency improvement, can solve problems such as alkali metal residues and safety hazards, avoid sodium-water reaction, improve safety, and reduce consumption. short time effect
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Embodiment A1
[0073] (1) Prepare dry ice: it consists of 25% by weight of Grade A dry ice, 25% by weight of Grade B dry ice and 50% by weight of Grade C dry ice.
[0074] (2) Alternately inject the first dry air flow and the second dry air flow into the pipeline, the carrier is nitrogen, the single injection time is 7s, and the interval is 3s;
[0075] The ice production speed is 0.06kg / s, and the carrier gas pressure is 0.78MPa;
[0076] The cleaned sodium and other impurities are blown out at the outlet and collected (sodium is mainly in the form of sodium carbonate), and the sodium content on the tube wall is detected by the detection head. When the sodium is cleaned, a total of 35 injections have been performed , the total amount of dry ice used is 14.5kg, and it takes 5min50s.
Embodiment A2
[0078] (1) Prepare dry ice: it is composed of 20% by weight of grade A dry ice, 25% by weight of grade B dry ice and 55% by weight of grade C dry ice.
[0079] (2) Alternately inject the first dry air flow and the second dry air flow into the pipeline, the carrier is nitrogen, the single injection time is 6s, and the interval is 4s;
[0080] The ice production speed is 0.05kg / s, and the carrier gas pressure is 0.65MPa;
[0081] When the sodium is cleaned, a total of 52 sprays are required, the total amount of dry ice is 15.5kg, and it takes 8min50s.
Embodiment A3
[0083] (1) Prepare dry ice: it is composed of 30% by weight of A-grade dry ice, 30% by weight of B-grade dry ice and 40% by weight of C-grade dry ice.
[0084] (2) Alternately inject the first dry air flow and the second dry air flow into the pipeline, the carrier is nitrogen, the single injection time is 8s, and the interval is 2s;
[0085] The ice production speed is 0.042kg / s, and the carrier gas pressure is 0.52MPa;
[0086] When the sodium is cleaned, a total of 50 sprays are required, the total amount of dry ice is 16.6kg, and it takes 8min15s.
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