Preparation method of kilometer-level multi-core MgB2 superconducting wire
A superconducting wire and wire technology, applied in the usage of superconducting elements, superconducting devices, superconducting/high-conducting conductors, etc., can solve problems such as uneven powder deformation, damage to metal sheath, and reduced wire transportation performance. , to achieve the effect of reducing deformation defects and uniform performance
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[0021] The invention provides a kilometer-level multi-core MgB 2 A method for preparing a superconducting wire, specifically comprising the following steps:
[0022] 1) Mix Mg powder and B powder according to the atomic ratio of 1:2, and grind to obtain precursor powder;
[0023] 2) Put the precursor powder into the Cu / Nb tube to assemble into Cu / Nb / MgB 2 Single mandrel, Cu / Nb / MgB by swaging 2 The single core rod is processed to the same size as the Cu center rod;
[0024] 3) Cu / Nb / MgB with the same size 2 The single mandrel and the Cu center rod are cut to length and cut in sequence, and put into the Monel tube to assemble into a multi-core composite sheath;
[0025] 4) The multi-core composite sheath is processed by swaging to obtain the finished wire rod;
[0026] 5) heat-treat the finished wire to obtain MgB 2 Multi-core superconducting wire.
[0027] Further, in step 2), Cu / Nb / MgB 2 The diameters of the single core rod and the Cu center rod are both Φ2.5mm~Φ6.0mm....
Embodiment 1
[0035] This embodiment provides a kilometer-level multi-core MgB 2 A method for preparing a superconducting wire, specifically comprising the steps of:
[0036] 1) Preparation of precursor powder: Weigh 353g of Mg powder and 343g of C-coated B powder in a glove box, mix Mg powder and B powder according to the atomic ratio of 1:2, and obtain the precursor powder after mechanical mixing for 20s;
[0037] 2) Preparation of single mandrel and center rod: the precursor powder is loaded into Cu / Nb tube to assemble Cu / Nb / MgB 2 Single mandrel, the single mandrel is processed to a diameter of 4.0mm by swaging; the Cu rod is processed to a diameter of 4.0mm by swaging to obtain a central rod;
[0038] 3) Preparation of 30+7-core composite sheath: the Cu / Nb / MgB prepared in step 2) 2 The single mandrel and the Cu center rod are cut into short rods with a length of 3m, where Cu / Nb / MgB 2 30 single mandrels and 7 Cu center rods are put into Monel tubes and assembled into 30+7 core composi...
Embodiment 2
[0043] This embodiment provides yet another kilometer-level multi-core MgB 2 A method for preparing a superconducting wire, specifically comprising the steps of:
[0044] 1) Preparation of precursor powder: Weigh 402g of Mg powder and 394g of C-coated B powder in the glove box, mix Mg powder and B powder according to the atomic ratio of 1:2, and obtain the precursor powder after mechanical mixing for 20s;
[0045] 2) Preparation of single mandrel and center rod: the precursor powder is loaded into Cu / Nb tube to assemble Cu / Nb / MgB 2 Single mandrel, the single mandrel is processed to a diameter of 6.0mm by swaging; the Cu rod is processed to a diameter of 6.0mm by swaging to obtain a center rod;
[0046] 3) Preparation of 18+1 core composite sheath: the Cu / Nb / MgB prepared in step 2) 2 The single mandrel and the Cu center rod are cut into short rods with a length of 2.5m, where Cu / Nb / MgB 2 18 single core rods, 1 Cu center rod, put into Monel tube, assembled into 18+1 core comp...
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