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Preparation method of dry strength agent for food-grade paper

A dry strength agent, food-grade technology, applied in the field of preparation of dry strength agent for food-grade paper, can solve the problem that the physical indicators such as paper folding endurance index, burst resistance index interlayer bonding strength and ring compressive strength are not significantly improved, and cannot be Guarantee the performance indicators and uneven quality of finished paper, and achieve the effect of improving mechanical strength, increasing bonding strength, and improving folding endurance index

Pending Publication Date: 2021-06-25
青州金昊新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Domestic waste paper has been reused many times, and the performance indicators of the finished paper cannot be guaranteed in terms of raw material structure and quality. For this, functional additives need to be added to improve its strength. However, the quality of paper strengthening agents on the market is uneven. It will cause fluctuations in the quality of the paper, and the physical indicators such as the folding index, bursting index, interlayer bonding strength and ring crushing strength of the paper after the use of the reinforcing agent have not been significantly improved. Therefore, we propose a food-grade Preparation method of dry strength agent for paper

Method used

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  • Preparation method of dry strength agent for food-grade paper

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A preparation method of a dry strength agent for food-grade paper, the above-mentioned production and its application are described in detail below:

[0029] (1) Prepare raw materials, 400 kg of acrylamide, 3 kg of anionic polymerizable monomer, 10 kg of cationic polymerizable monomer, 0.1 kg of chelating agent, 0.5 kg of inorganic acid, 1 kg of molecular weight regulator, 0.3 kg of initiator, and 0.5 kg of terminator kg, 584.6 kg of deionized water;

[0030] (2) Add amide solution, anionic and cationic polymerizable monomers, chelating agent, inorganic acid, molecular weight modifier and half of the amount of deionized water in the reaction kettle, stir evenly, the stirring speed is 20r / m, and turn out 50% with a metering pump Material is added in dripping kettle A;

[0031] (3) Nitrogen gas exhausts oxygen, and the reaction kettle is heated up to 60°C;

[0032] (4) configuration initiator solution concentration is 2%, changes over to dripping still B;

[0033] (5) ...

Embodiment 2

[0048] A preparation method of a dry strength agent for food-grade paper, the above-mentioned production and its application are described in detail below:

[0049] (1) Prepare raw materials, 480 kg of acrylamide, 6 kg of anionic polymerizable monomer, 20 kg of cationic polymerizable monomer, 0.3 kg of chelating agent, 1.2 kg of inorganic acid, 3 kg of molecular weight regulator, 0.6 kg of initiator, and 1 kg of terminator kg, 487.9 kg of deionized water;

[0050] (2) Add amide solution, anionic and cationic polymerizable monomers, chelating agent, inorganic acid, molecular weight modifier and half of the amount of deionized water in the reaction kettle, stir evenly, the stirring speed is 35r / m, and turn out 50% with a metering pump Material is added in dripping kettle A;

[0051] (3) Nitrogen exhaust, and the reaction kettle is heated up to 75°C;

[0052] (4) configuration initiator solution concentration is 3%, changes over to dripping still B;

[0053] (5) the concentrat...

Embodiment 3

[0068] A preparation method of a dry strength agent for food-grade paper, the above-mentioned production and its application are described in detail below:

[0069] (1) Prepare raw materials, 550 kg of acrylamide, 10 kg of anionic polymerizable monomer, 30 kg of cationic polymerizable monomer, 0.5 kg of chelating agent, 2 kg of inorganic acid, 5 kg of molecular weight regulator, 1 kg of initiator, and 1.5 kg of terminator kg, 400 kg of deionized water;

[0070] (2) Add amide solution, anionic and cationic polymerizable monomers, chelating agent, inorganic acid, molecular weight modifier and half of the amount of deionized water in the reaction kettle, stir evenly, and the stirring speed is 50r / m, and turn out 50% with a metering pump Material is added in dripping kettle A;

[0071] (3) Nitrogen gas exhausts oxygen, and the reaction kettle is heated up to 90°C;

[0072] (4) configuration initiator solution concentration is 4%, changes over to dripping still B;

[0073] (5) t...

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Abstract

The invention discloses a preparation method of a dry strength agent for food-grade paper, which comprises the following steps: (1) preparing the following raw materials in parts by weight: 40-55 parts of acrylamide, 0.3-1 part of anionic polymerization monomer, 1-3 parts of cationic polymerization monomer, 0.01-0.05 part of chelating agent, 0.05-0.2 part of inorganic acid, 0.1-0.5 part of molecular weight regulator, 0.03-0.1 part of initiator, 0.05-0.15 part of terminator and 40-60 parts of deionized water; and (2) adding an amide solution, anionic and cationic polymerization monomers, a chelating agent, inorganic acid, a molecular weight regulator and half of deionized water into a reaction kettle, and uniformly conducting stirring. According to the preparation method of the dry strength agent for the food-grade paper, the residual amount of the acrylamide monomer of the dry strength agent for the food-grade paper is less than 0.001%, and the dry strength agent can be safely suitable for the processes of production and manufacturing of the food paper, subsequent food processing and packaging and the like. The product can effectively increase the bonding area and bonding strength among fibers in papermaking paper under the condition of ensuring food safety, effective hydrogen bonding is formed, and the mechanical strength of the paper is remarkably improved.

Description

technical field [0001] The invention relates to the technical field of chemical industry, in particular to a preparation method of a dry strength agent for food-grade paper. Background technique [0002] Paper is the most commonly used item in people's daily life. With the advancement of science and technology and the upgrading of consumer demand, the market demand for paper is increasingly showing trends such as individualized demand, specialized application, large-scale supply and resource recycling. The corresponding papermaking industry will also develop towards enterprise scale, technology integration, product diversification, production cleanliness, resource conservation, forestry and paper integration and industrial globalization. my country's packaging paper mainly uses waste paper as raw material for production. The main waste paper importing countries are the United States, the United Kingdom, and Japan. The United States is the main source. The waste paper market is...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F220/56C08F220/06C08F222/02C08F228/02C08F220/34D21H17/37D21H17/43D21H17/45D21H21/18
CPCC08F220/56D21H17/375D21H17/43D21H17/455D21H21/18
Inventor 曹玉岗赵海刚张云英
Owner 青州金昊新材料有限公司
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