Rapid repair adhesive as well as preparation method and application method thereof
An adhesive and fast technology, used in sustainable waste treatment, solid waste management, pavement detailing, etc., can solve the problems of slow curing speed, long closed traffic time, curing speed to be improved, etc., to achieve fast curing speed, Increase the effect of compactness and high flatness
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preparation example 1-6
[0043] The EVA powder in the preparation example 1-6 is selected from Dongguan Xiegang Lianfa Plastic Raw Material Management Department, the model is 150W, and its performance parameters are shown in Table 1; the emulsifier is selected from Guangzhou Zhanlin Chemical Co., Ltd., the model is NP-10 ; Waste tire rubber powder is selected from Lingshou County Detong Mineral Products Processing Plant, the model is DT-XJ71; silane coupling agent KH570 is selected from Qingdao Xuxin Chemical Co., Ltd.; bisphenol F epoxy resin is selected from Shanghai Fanxiao Chemical Technology Ltd., model number F170.
[0044] Table 1 Performance parameters of EVA powder
[0045]
preparation example 1
[0046] Preparation Example 1: (1) Mix 10kg of waste tire rubber powder with 20kg of sodium hypochlorite with a concentration of 15%, stir at 60°C for 30min, filter, wash until neutral, and dry at 75°C for 6h to obtain activated rubber powder. The particle size of tire rubber powder is 80 mesh;
[0047] (2) Mix activated rubber powder, 4kg silane coupling agent KH570, 2kg bisphenol F epoxy resin and 0.5kg ammonium persulfate, stir evenly, and obtain the capsule core material;
[0048] (3) Mix EVA powder and emulsifier, raise the temperature to 100°C, adjust the pH to 7, mix with the capsule core material, stir evenly, adjust the pH to 4 with dilute hydrochloric acid, filter, wash, and dry to make rubber powder, 10kg Capsule core material and 2kg EVA powder, emulsifier dosage is 0.4k.
preparation example 2
[0049] Preparation Example 2: (1) Mix 13kg of waste tire rubber powder with 23kg of sodium hypochlorite with a concentration of 18%, stir at 70°C for 25min, filter, wash until neutral, and dry at 80°C for 5h to obtain activated rubber powder. The particle size of tire rubber powder is 80 mesh;
[0050] (2) Mix activated rubber powder, 6kg silane coupling agent KH570, 2.5kg bisphenol F epoxy resin and 0.8kg ammonium persulfate, stir evenly, and obtain the capsule core material;
[0051] (3) Mix EVA powder and emulsifier, raise the temperature to 120°C, adjust the pH to 7, mix with the capsule core material, stir evenly, adjust the pH to 4 with dilute hydrochloric acid, filter, wash, and dry to make rubber powder, 15kg Capsule core material and 4.5kg EVA powder, emulsifier dosage is 0.6k.
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