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Calibration method of thin film thermal resistance heat flow meter and coaxial thermocouple for heat flow test

A calibration method and thermal resistance technology, applied in thermometer testing/calibration, thermometers, calorimeters, etc., can solve problems such as inaccurate heat flow results, achieve reliable test result uncertainty evaluation results, and clarify the need for traceability of quantities Effect

Active Publication Date: 2021-07-27
中国空气动力研究与发展中心超高速空气动力研究所
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Obviously, the product of pyroelectric coefficient and thermophysical parameter determined by this two-step method will inevitably introduce more error factors when evaluating the uncertainty of heat flow test results
At the same time, some literature pointed out that the heat flow results estimated by the Cook-Feldeman method are not accurate enough, and the Cook-Feldeman method is often used when estimating the effective thermophysical parameter product

Method used

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  • Calibration method of thin film thermal resistance heat flow meter and coaxial thermocouple for heat flow test
  • Calibration method of thin film thermal resistance heat flow meter and coaxial thermocouple for heat flow test
  • Calibration method of thin film thermal resistance heat flow meter and coaxial thermocouple for heat flow test

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0048] To calibrate a thin film thermal resistance heat flow meter, the calibration steps include:

[0049] Step 1. Check the heat flow sensor calibration equipment, determine the calibration heat flow range, and select 5 different calibration heat flow points, and use the atomic layer thermopile heat flow sensor to check the stability of the calibration heat flow in time;

[0050] Step 2. Spray a layer of carbon black coating on the surface of the thin film thermal resistance heat flow meter to be calibrated, the coating thickness is not more than 1 μm; the coating material can also be one of colloidal graphite, gold black or platinum black; The base material of the resistance heat flow meter is polyimide, and polyether ether ketone can also be used; when the base material of the thin film heat resistance heat flow meter is glass or ceramics, a layer of diamond film should be deposited on the sensing surface of the thin film heat resistance heat flow meter, thus Other coating...

Embodiment 2

[0066] To calibrate a coaxial thermocouple, the calibration steps include:

[0067] Step 1. Check the heat flow sensor calibration equipment, determine the calibration heat flow range, and select 5 different calibration heat flow points, and use the atomic layer thermopile heat flow sensor to check the stability of the calibration heat flow in time;

[0068] Step 2. Spray a layer of carbon black coating on the surface of the coaxial thermocouple to be calibrated. The coating can also be one of gold black, colloidal graphite or platinum black coating, and the coating thickness does not exceed 1 μm;

[0069] Step 3. Fix the coaxial thermocouple to be calibrated at the designated position of the heat flow sensor calibration equipment;

[0070] Step 4, set the parameters of the function generator and the dynamic data acquisition instrument, turn on the fiber laser and the dynamic data acquisition instrument, and obtain the output of the coaxial thermocouple under a certain calibra...

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Abstract

The invention discloses a calibration method of a thin film thermal resistance heat flow meter and a coaxial thermocouple for a heat flow test. The method comprises the steps: determining a calibration heat flow range, and selecting a calibration heat flow value; spraying a coating on the surface of the heat flow sensor; acquiring the output of the heat flow sensor under a certain calibration heat flow; moving the heat flow sensor out of a calibration position, fixing a water-cooling Gardon meter, and acquiring the output of the water-cooling Gardon meter; acquiring the outputs of the heat flow sensor to be calibrated and the water-cooling Gardon meter under a series of calibration heat flows; processing the heat flow sensor output to obtain an output average value; calculating the input heat flow of the heat flow sensor by using the nominal sensitivity coefficient of the water-cooling Gardon meter and the output under a certain calibration heat flow and combining the absorptivity of the surface coating of the heat flow sensor; and fitting the average values output by the multiple pairs of heat flow sensors and the input heat flow by using a least square method to obtain the sensitivity coefficient of the heat flow sensors. According to the method, the requirement of a heat flow sensor test value for definite value traceability is met, and a reliable uncertainty evaluation result is provided.

Description

technical field [0001] The invention belongs to the technical field of heat flow sensor calibration, and more specifically relates to a method for calibrating a thin-film thermal resistance heat flow meter and a coaxial thermocouple used for heat flow testing. Background technique [0002] At present, in pulsed wind tunnels such as shock wave wind tunnels, heat flow tests are mainly carried out by using thin film thermal resistors and coaxial thermocouples. When using thin film thermal resistance or coaxial thermocouple to carry out heat flow test, the surface temperature obtained by these two sensors is used to obtain the heat flow test result by inversion. The difference is that the thin film thermal resistance uses the linear dependence between the resistance and temperature of the platinum metal thin film to achieve temperature testing, while the coaxial thermocouple uses the Seebeck effect of different thermocouple materials to obtain the surface temperature test result...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01K19/00G01K15/00
CPCG01K19/00G01K15/007Y02E30/30
Inventor 杨凯陈苏宇李强朱新新王辉杨远剑
Owner 中国空气动力研究与发展中心超高速空气动力研究所
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