Portable photothermal seawater desalination hollow fiber membrane, preparation method, device and application
A fiber membrane and portable technology, applied in the field of portable photothermal seawater desalination hollow fiber membrane and its preparation, can solve the problems of unavoidable heat loss, limited wide use, low photothermal efficiency, etc., and achieve uniform black appearance, excellent mechanical strength, The effect of high specific surface area
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Embodiment 1
[0064] First of all, Example 1 provides a preparation method of a photothermal seawater desalination hollow fiber membrane: an ultra-thin film with an average pore size of 0.9 μm, a porosity of 60%, a membrane thickness of 200 μm, and an inner / outer diameter of 0.5 mm / 1.0 mm is used. The hydrophilic polysulfone hollow fiber gradient membrane was used as a polymer-based membrane, and the 0.5 wt% carbon nanotube dispersion was fixed on the outer surface of the hollow fiber membrane by surface adsorption by vacuum filtration technology for 1 h, and the outer surface had photothermal function. The hollow fiber membrane with black appearance of the layer can be obtained after cleaning and drying.
[0065] The polymer hollow fiber membrane modified by carbon nanotubes has excellent self-siphoning performance, and the appearance is uniform black. Secondly, this embodiment 1 also provides a portable photothermal seawater desalination device. The operation method is as follows: One end...
Embodiment 2
[0067] First, Example 2 provides a preparation method of a photothermal seawater desalination hollow fiber membrane: Step 1: adopt an average pore diameter of 2 μm, a porosity of 80%, a membrane thickness of 50 μm, and an inner / outer diameter of 0.1 mm / 0.25 mm, respectively. The hydrophobic polyethylene hollow fiber membrane is a polymer-based membrane, and dopamine and polyethyleneimine are dispersed and dissolved in a buffer solution with a pH of 8.5 to configure a homogeneous solution, wherein the ratio of dopamine:polyethyleneimine is 1:1; The surface coating technology is treated for 12h so that the homogeneous solution is fixed on the inner surface of the hollow fiber membrane, cleaned and dried for later use;
[0068] Step 2: The polymer base membrane treated in Step 1 is placed in a 2wt% polypyrrole solution for outer surface vapor deposition modification for 3 hours to obtain a black-looking hollow fiber membrane with a photothermal functional layer on the outer surfac...
Embodiment 3
[0072] First of all, Example 3 provides a preparation method of a photothermal seawater desalination hollow fiber membrane: an ultra-thin film with an average pore size of 1.0 μm, a porosity of 40%, a membrane thickness of 200 μm, and an inner / outer diameter of 2.0 mm / 3.5 mm is used. The hydrophilic polyethersulfone hollow fiber membrane is a polymer-based membrane. The superhydrophilic polyethersulfone hollow fiber membrane was placed in a 20 wt% polyaniline solution for cross-linking fixation and modification on the outer surface for 6 h. The black appearance hollow fiber membrane of the thermal functional layer can be washed and dried to obtain the hollow fiber membrane of photothermal seawater desalination. The polyaniline-modified polymer hollow fiber membrane prepared in Example 3 has excellent self-siphoning performance, and the appearance is uniform black.
[0073]Secondly, this embodiment 3 also provides a portable photothermal seawater desalination device, and the op...
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