A kind of metal roof thermal insulation waterproof coating and preparation method thereof
A technology for metal roofing and waterproof coatings, applied in the direction of reflection/signal coatings, chloroprene homopolymer coatings, coatings, etc., can solve the problem of low tensile strength retention rate, no heat resistance, Easy aging and other problems, to achieve the effect of improving stability and heat insulation effect, improving permeability and leveling, and improving tensile strength retention rate
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preparation example 1
[0040] Preparation examples 1-8 provide a silicone-modified hollow glass microsphere, and preparation example 1 is taken as an example for illustration below.
[0041] The organosilicon modified hollow glass microspheres provided by Preparation Example 1, its preparation steps are:
[0042] (1) Add 500L aqueous sodium hydroxide solution with a concentration of 0.2mol / L to 10kg hollow glass microspheres, react at 75°C for 2h, wash with deionized water until neutral, filter with suction, take the solid, and dry the solid at 80°C , to obtain hydroxylated hollow glass microspheres;
[0043] (2) Add 400L of ethanol aqueous solution with a volume ratio of 1:3 to the hydroxylated hollow glass microspheres prepared in step S1, and then add 2kg of 1,3-divinyltetraethoxydisilane (CAS No. 3682-26- 6) and 1kg 3-mercaptopropyltrimethoxysilane (CAS No. 4420-74-0), reacted at 80°C for 4h, suction filtered after the reaction, washed the solid with ethanol 5 times, and put the washed solid at...
preparation example 6
[0047] Preparation Example 6 differs from Preparation Example 1 only in that: the equivalent mass of 1,3-divinyltetraethoxydisilane is replaced by 3-mercaptopropyltrimethoxysilane.
preparation example 7
[0048] Preparation Example 7 differs from Preparation Example 1 only in that: the equivalent mass of 3-mercaptopropyltrimethoxysilane is replaced by 1,3-divinyltetraethoxydisilane.
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