Preparation method of thermally induced flexible phase change energy storage wood
A phase change energy storage and thermal induction technology, applied in wood treatment, wood impregnation, wood impregnation, etc., can solve the problems of easy leakage, poor material flexibility, low thermal conductivity, etc., achieving low cost, long service life, and improved thermal conductivity. The effect of coefficients
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Embodiment 1
[0023] Embodiment 1: A kind of preparation method of heat-induced flexible phase change energy storage wood, balsa wood with a thickness of 2mm is processed, cut into length×width 40mm×20mm wood chips for later use, and proceed according to the following steps:
[0024] a, with N,N dimethylformamide as solvent, configure 0.08mol / L triethanolamine solution 53g and 0.3mol / L triphenylmethane triisocyanate solution 45g;
[0025] b. Add the triethanolamine solution in step a to the triphenylmethane triisocyanate solution, and stir at 75°C for 12 hours to obtain a prepolymer;
[0026] c. Add 13 g of polyethylene glycol-1500 to the prepolymer, and stir at 75° C. for 28 hours to obtain a solid-solid phase change material;
[0027] d. Put the delignified wood into the solid-solid phase change material, vacuum impregnate (0.1MPa) for 25 minutes, and then dry to obtain the finished product.
Embodiment 2
[0028] Embodiment 2: A kind of preparation method of heat-induced flexible phase change energy storage wood, balsa wood with a thickness of 2mm is processed, cut into length×width 40mm×20mm wood chips for later use, and proceed according to the following steps:
[0029] a, with N,N dimethylformamide as solvent, configure 0.15mol / L triethanolamine solution 65g and 0.2mol / L triphenylmethane triisocyanate solution 55g;
[0030] b. Add the triethanolamine solution in step a to the triphenylmethane triisocyanate solution, and stir at 65°C for 15 hours to obtain a prepolymer;
[0031] c. Add 18 g of polyethylene glycol-1500 to the prepolymer, and stir at 65° C. for 25 hours to obtain a solid-solid phase change material;
[0032] d. Put the delignified wood into the solid-solid phase change material, vacuum impregnate (0.1MPa) for 35 minutes, and then dry to obtain the finished product.
Embodiment 3
[0033] Embodiment 3: A kind of preparation method of heat-induced flexible phase change energy storage wood, balsa wood with a thickness of 2mm is processed, cut into length×width 40mm×20mm wood chips for later use, and proceed according to the following steps:
[0034] a, with N,N dimethylformamide as solvent, configure 0.1mol / L triethanolamine solution 58g and 0.27mol / L triphenylmethane triisocyanate solution 48g;
[0035] b. Add the triethanolamine solution in step a to the triphenylmethane triisocyanate solution, and stir at 70°C for 12 hours to obtain a prepolymer;
[0036] c. Add 15 g of polyethylene glycol-1500 to the prepolymer, and stir at 70° C. for 24 hours to obtain a solid-solid phase change material;
[0037] d. Put the delignified wood into the solid-solid phase change material, vacuum impregnate (0.1MPa) for 30 minutes, and then dry to obtain the finished product.
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