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Novel filtering, washing and drying integrated device and process

A technology for washing, drying, and integrating devices. It is used in filtration and separation, drying chambers/containers, and drying solid materials. It can solve problems such as changing crystal morphology, blocking exhaust traps, and destroying material crystal forms.

Active Publication Date: 2021-08-31
上海迪化科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There must be a layer of material in the gap, which brings five problems: one is to form a dead zone during the washing process, which affects the washing efficiency; the other is to affect the heat exchange efficiency between the material and the wall and reduce the drying efficiency; The radial temperature is not uniform, resulting in uneven product quality (the temperature near the wall is the highest, and the center temperature is the lowest); the fourth is that there are residual materials during unloading, and the discharge is incomplete, which affects the yield or causes mixed batch pollution; fifth, in the Under the mechanical force of stirring, cutting, shearing or extrusion, it is easy to cause the material to break, pulverize or change the crystal form
[0006] (2) The drying process is heated by the heat medium in the equipment jacket, which belongs to heat conduction heating. Compared with the convection drying process, the drying efficiency is significantly reduced
[0007] (3) The existing "three-in-one" is equipped with a solid particle trap at the gas outlet to intercept the solid powder entrained by the air flow, but because the filter area is small, the exhaust trap is often blocked, even if the exhaust filter The outlet is equipped with a back-blowing system, and the blown-off material has not waited to fall to the main material layer, but is quickly brought to the trap by the rising airflow, causing repeated clogging of the filter, and the more serious it is in the later stage of drying
[0008] In short, because the existing "three-in-one" filtration process is static filtration, there is a dead zone in the washing process, and the drying process relies on heat conduction heating and stirring to crush the material, resulting in low production efficiency, uneven product quality, and easy blockage of the filter screen. Problems such as destroying the crystal form of materials and low degree of automation, therefore, limit the promotion and application of "three-in-one" in certain fields and certain products

Method used

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  • Novel filtering, washing and drying integrated device and process
  • Novel filtering, washing and drying integrated device and process
  • Novel filtering, washing and drying integrated device and process

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0112] Such as Figure 1-5 A novel filter, washing and drying integrated device shown includes a drum 1, a rotating shaft 2, a gas-liquid distribution system 3, and a rotary joint 4; the drum 1 and the rotating shaft 2 are coaxially fixedly connected; the rotating shaft 2 It is connected with the gas-liquid distribution system 3 through the rotary joint 4;

[0113] The rotary joint 4 includes a dynamic ring joint 41 and a static ring joint 42; the static ring joint 42 is divided into an upper half and a lower half, and the upper and lower halves of the static ring joint 42 are independent of each other; The ring joint 41 is arranged on the rotating shaft 2 and rotates synchronously with the rotating shaft 2. The static ring joint 42 is arranged in the gas-liquid distribution system 3 and is relatively stationary with the gas-liquid distribution system 3. The moving ring joint 41 is arranged opposite to the static ring joint 42;

[0114] A gas-liquid channel 21 is arranged in...

Embodiment 2

[0121] Based on the filtration process of the novel filter washing and drying integrated device provided in embodiment 1, comprise the following steps:

[0122] S1-1: Open the valve 36 between the mother liquor tank 32 and the vacuum tank 33;

[0123] S1-2: Open the valve 36 between the lower half of the static ring joint 42 and the mother liquid tank 32;

[0124] S1-3: Close the remaining valves 36; pump the filtered mother liquor into the mother liquor tank 32 by vacuum, and solids are intercepted by the filter screen 12 in the drum 1 .

Embodiment 3

[0126] Based on the intermittent washing process of the novel filter washing and drying integrated device provided in embodiment 1, it may further comprise the steps:

[0127] S2-1: stop the rotation of the drum 1, and open the valve 36 between the static ring joint 42 and the booster pump 37;

[0128] S2-2: add detergent into the drum 1 through the booster pump 37, and control the material level to not exceed two-thirds of the vertical height of the drum 1;

[0129] S2-3: Control the rotation of the drum 1, the materials in the drum 1 are turned accordingly, and the materials fully contact with the detergent;

[0130] S2-4: Adjust the rotation speed and washing time of the drum 1 according to the material properties and washing requirements.

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PUM

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Abstract

The invention belongs to the technical field of process equipment, in particular to a novel filtering, washing and drying integrated device and a process. The novel filtering, washing and drying integrated device comprises a roller, a rotary shaft, a gas-liquid distribution system and a process control system, wherein the roller is coaxially and fixedly connected with the rotary shaft; and the roller and the gas-liquid distribution system are connected through a rotating joint. According to the novel filtering, washing and drying integrated device provided by the invention, the processes of filtering, washing and drying are completely carried out in one device, and thus, the production efficiency is high, dead angles are avoided, uniform quality of products is realized, material breakage ratios are low, the device conforms to the GMP (Good Manufacturing Practices) sanitary standard, and the automation level is high.

Description

technical field [0001] The invention belongs to the technical field of process equipment, and in particular relates to a novel filtering, washing and drying integrated device and process. Background technique [0002] Traditionally, the three processes of filtration, washing and drying are completed independently in unit equipment such as centrifuge (or filter), washing kettle (trough), dryer (or oven), and the integrated filtering, washing and drying machine (commonly known as "three "In one", hereinafter referred to as "three in one") has the ability to complete from feeding to product discharge in one equipment, reducing the number of equipment and space occupation, reducing labor intensity, reducing material pollution by people and the environment during the process, etc. Therefore, it has been widely used in chemical industry, medicine, light industry, biology, traditional Chinese medicine, food, agricultural product processing and other fields in recent years. [0003...

Claims

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Application Information

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IPC IPC(8): F26B5/04F26B11/04F26B25/16F26B3/08B01D29/03B08B3/04B08B3/14B08B13/00
CPCF26B5/04F26B11/04F26B25/16F26B3/08B01D29/03B08B3/044B08B3/14B08B13/00
Inventor 梁万义梁育阁
Owner 上海迪化科技股份有限公司
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