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UV printing ink and preparation method thereof

An ink, epoxy acrylate technology, applied in the direction of ink, household appliances, applications, etc., can solve the problems of affecting the curing effect, high ink viscosity, insufficient adhesion and flexibility, etc., to promote hardening rate, fast curing rate, curing The effect of reducing the effect

Pending Publication Date: 2021-09-21
东莞市彩工坊新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, most of the existing UV inks are dried on the surface due to the obstruction of light on the surface of the film layer, which affects the overall curing effect, and the adhesion and flexibility are insufficient, and the viscosity of the ink is too high, which is difficult to meet customer needs.

Method used

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  • UV printing ink and preparation method thereof
  • UV printing ink and preparation method thereof
  • UV printing ink and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A kind of UV printing ink, comprises the raw material of following weight part:

[0037]

[0038] The preparation method of described epoxy acrylate comprises the steps:

[0039] (R1), get 100 parts of epoxy resin, 35 parts of acrylic acid, 0.03 part of hydroquinone, 0.08 part of triethylamine and 20 parts of vinyl alkoxysilane oligomers by weight, for subsequent use;

[0040] (R2), after mixing acrylic acid, hydroquinone and triethylamine, a mixed solution is obtained;

[0041] (R3) Stir the epoxy resin and heat it up to 95°C, then continue to drop the mixed solution, and react at a temperature of 115°C for 3 hours to obtain a semi-finished product;

[0042] (R4), add vinyl alkoxy silane oligomer to the semi-finished product, then stir and react at 80°C for 1.5h under the catalysis of organotin, distill under reduced pressure, then wash, dry and filter to obtain epoxy acrylic acid ester.

[0043] The epoxy resin is EP-12; the vinyl alkoxy silane oligomer is selec...

Embodiment 2

[0055] A kind of UV printing ink, comprises the raw material of following weight part:

[0056]

[0057] The preparation method of described epoxy acrylate comprises the steps:

[0058] (R1), get 100 parts of epoxy resin, 33 parts of acrylic acid, 0.01 part of hydroquinone, 0.05 part of triethylamine and 10 parts of vinyl alkoxysilane oligomers by weight, for subsequent use;

[0059] (R2), after mixing acrylic acid, hydroquinone and triethylamine, a mixed solution is obtained;

[0060] (R3) Stir the epoxy resin and raise the temperature to 90°C, then continue to drop the mixed solution, and react at a temperature of 110°C for 2 hours to obtain a semi-finished product;

[0061] (R4), adding vinyl alkoxysilane oligomer to the semi-finished product, then stirring and reacting for 0.5h at 50°C under the catalysis of organotin, distilling under reduced pressure, washing, drying and filtering to obtain epoxy acrylic acid ester.

[0062] The epoxy resin is EP-16; the vinyl alko...

Embodiment 3

[0073] A kind of UV printing ink, comprises the raw material of following weight part:

[0074]

[0075]

[0076] The preparation method of described epoxy acrylate comprises the steps:

[0077] (R1), get 100 parts of epoxy resin, 36 parts of acrylic acid, 0.05 part of hydroquinone, 0.1 part of triethylamine and 30 parts of vinyl alkoxysilane oligomers by weight, for subsequent use;

[0078] (R2), after mixing acrylic acid, hydroquinone and triethylamine, a mixed solution is obtained;

[0079] (R3) Stir the epoxy resin and heat it up to 100°C, then continue to drop the mixed solution, and react at a temperature of 120°C for 4 hours to obtain a semi-finished product;

[0080] (R4), add vinyl alkoxysilane oligomer to the semi-finished product, then stir and react at 100°C for 3 hours under the catalysis of organotin, distill under reduced pressure, then wash, dry and filter to obtain epoxy acrylate .

[0081] The epoxy resin is EP-16; the vinyl alkoxy silane oligomer is...

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Abstract

The invention relates to the technical field of UV ink, in particular to UV ink and a preparation method thereof. The UV ink is prepared from the following raw materials in parts by weight: 50 to 70 parts of epoxy acrylate, 10 to 15 parts of polyester acrylate, 4 to 8 parts of polydiallyl phthalate, 3 to 5 parts of a photoinitiator, 2 to 3 parts of a photosensitizer, 15 to 25 parts of a reactive diluent, 5 to 10 parts of diatomite, 0.2 to 0.5 part of a defoaming agent, 1 to 2 parts of polyethylene wax, 2 to 4 parts of a dispersing agent and 0 to 20 parts of a coloring agent. Through the synergistic effect, the overall adhesiveness, the flexibility, the wear resistance and the curing effect of the UV ink are improved, and the viscosity is reduced.

Description

technical field [0001] The invention relates to the technical field of UV ink, in particular to a UV ink and a preparation method thereof. Background technique [0002] UV (ultraviolet curing) ink refers to the ink that uses ultraviolet light of different wavelengths and energies to polymerize the monomers in the ink binder into polymers to form a film and dry the ink under ultraviolet radiation. UV inks are also inks. As inks, they must have bright colors (except in special cases), good printability, and suitable curing and drying rates. However, most of the existing UV inks are dried on the surface due to the obstruction of light on the surface of the film layer, which affects the overall curing effect, and the adhesion and flexibility are insufficient, and the viscosity of the ink is too high, which is difficult to meet customer needs. Contents of the invention [0003] In order to overcome the shortcomings and deficiencies in the prior art, the object of the present i...

Claims

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Application Information

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IPC IPC(8): C09D11/101C09D11/03
CPCC09D11/101C09D11/03Y02P20/10
Inventor 黄劲涛刘志健林应森
Owner 东莞市彩工坊新材料有限公司
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