Diamine derivative for organic electroluminescent device
An electroluminescent device, a technology of diamine derivatives, applied in the field of semiconductors, can solve the problems of short life and high voltage, achieve the effect of improving hole injection efficiency and reducing the risk of Cross-talk
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[0038] Example 1: Synthesis of Compound 1:
[0039]
[0040] 250ml three-necked flask, under the atmosphere of nitrogen, add 0.01mol raw material A-1, 0.012mol raw material B-1, 0.03mol potassium tert-butoxide, 1×10 -4 mol pd 2 (dba) 3 , 1 × 10 -4 mol triphenylphosphine, 150 ml of toluene, heated to reflux for 12 hours, sampling point plate, the reaction was complete; naturally cooled, filtered, the filtrate was rotary evaporated, passed through a silica gel column to obtain intermediate D-1; elemental analysis structure (molecular formula C 34 H 24 ClN): Theoretical C, 84.72; H, 5.02; N, 7.35; Cl, 2.91; found: C, 84.75; H, 5.01; N, 7.34; Cl, 2.90. ESI-MS(m / z)(M + ): The theoretical value is 481.16, and the measured value is 481.32.
[0041] In a 250ml three-necked bottle, under a nitrogen atmosphere, add 0.01mol of intermediate D-1, 0.012mol of raw material C-1, 0.03mol of potassium tert-butoxide, 1×10 -4 mol pd 2 (dba) 3 , 1 × 10 -4mol triphenylphosphine, 15...
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