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Raman spectrometer measurement environment control method and system

A Raman spectrometer and ring-shaped technology, which is applied in the field of mud logging gas composition detection, can solve problems such as difficulty in implementation, impact on detection results, and difficulties

Pending Publication Date: 2021-10-22
中石化石油工程技术服务有限公司 +3
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Problems solved by technology

In mud logging, mud logging gas flows at a high speed and its composition changes in real time. Its thermal conductivity and heat capacity are much lower than those of metals. It will be very difficult to make it heat up rapidly and keep a constant temperature in a limited space and a very high sample flow rate. Combined with Flowing gas pressure control, purification treatment and other procedures, the realization of the whole system is full of difficulties
[0004] To sum up, in order to realize the application of Raman spectrometer in the field of field logging and gas logging, it is necessary to solve the problem that the measurement environment affects the detection results

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  • Raman spectrometer measurement environment control method and system
  • Raman spectrometer measurement environment control method and system
  • Raman spectrometer measurement environment control method and system

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Embodiment

[0100] Under different altitudes / different atmospheric pressure environments, different relative pressures, and different absolute pressures, the temperature of the optical path cell is set at 50°C, and the temperature of the gas entering the optical path cell is set at 50°C. After about 60 minutes of preheating, the temperature of the optical path cell, The temperature of the gas entering the optical path cell body 230 is constant at 50±0.5° C., and six standard gases of different types and concentrations are pumped into the Raman instrument for analysis.

[0101] 1. Experimental location:

[0102] ① Feiniuba Village, Yongxing Town, Mianyang: Altitude 476m, atmospheric pressure 95.941Kpa; ② Suburbs of Kangding: Altitude 2292m, atmospheric pressure 77.170-77.181Kpa; ③ Zhonggu Village, Yala Mountain, Kangding: Altitude 2980m, atmospheric pressure 70.74Kpa.

[0103] 2. Pressure parameters: ①Analyze at normal pressure at the above three experimental locations; ②Analyze at constan...

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Abstract

The invention provides a Raman spectrometer measurement environment control method and system. The system comprises a Raman spectrometer temperature control system and a sample purification and flow and pressure control system. The Raman instrument temperature control system comprises a Raman spectrometer sample gas micro heater, a heat conductor temperature measuring meter, a gas temperature measuring tee joint, a gas temperature measuring meter, a Raman instrument optical path pool body, an optical path pool body temperature measuring meter, a temperature setting instrument, a PID (Proportion Integration Differentiation) operation program device, a regulator, a heater temperature controller and an optical path pool temperature controller. According to the scheme, the problems that a Raman spectrometer cannot adapt to the severe and changeable logging site environment, and the measured value is inaccurate can be solved.

Description

technical field [0001] The invention belongs to the field of mud logging gas component detection, and in particular relates to a method and system for controlling the temperature, pressure and flow of high-speed flowing gas, thereby realizing the unification of the measurement environment of a Raman spectrometer under various mud logging site conditions. Background technique [0002] Gas logging is the core technology of mud logging and the most direct and effective means to discover oil and gas layers. Its detection technologies are mainly hydrogen flame chromatography technology, thermal conductivity chromatography technology, and infrared spectroscopy technology. Due to their shortcomings such as long detection period, few detection indicators, and recalibration and correction when changing well positions, it is becoming more and more difficult to adapt to the complex oil and gas at the present stage. Tibet exploration work requirements. Raman spectroscopy has become one...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/65G01N21/01G01N1/28G01N1/34G01N1/44G05D27/02
CPCG01N21/65G01N21/01G01N1/28G01N1/34G01N1/44G05D27/02
Inventor 胡昌平梁波夏杰王崇敬颜磊吴桐权杨刘云朱潇王超潘晓东唐诚王政廖震徐冬莲陈琪郭同兵刘福文闫光辉杨立会王春李晋周瑜王萍李锐强青羿唐永兵肖军赵川杨旭东李红强曲文波蔡欢欢宋飞鹏王利福张勇
Owner 中石化石油工程技术服务有限公司
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