Method for preventing edge dislocation of silicon carbide crystal from slipping inwards
An edge dislocation, silicon carbide technology, applied in chemical instruments and methods, crystal growth, single crystal growth and other directions, to achieve the effect of improving crystal quality, simple operation, good repeatability and stability
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Embodiment 1
[0065] This embodiment provides a method for blocking edge dislocations and blocking edge dislocations of silicon carbide crystals from slipping inward, the method comprising the following steps:
[0066] Step 1. Place the crucible containing 1 kg of silicon carbide powder and a 4-inch silicon carbide seed crystal fixed on the crucible cover in the above-mentioned heat preservation cover, and then place the crucible together with the heat preservation cover in the growth chamber of the crystal growth furnace, that is, the structure Such as figure 1 The thermal field shown;
[0067] Step 2. Control the temperature and pressure of the crystal growth furnace and the flow of inert gas into the crystal growth furnace to clean and remove impurities in the crystal growth furnace, and then use the crystal growth furnace to grow crystals, specifically including the following stages:
[0068] Heating stage: adjust the temperature of the crystal growth furnace to 2000-2400K, and control...
Embodiment 2~8
[0073] The preparation methods of Examples 2-8 are roughly the same as those of Example 1, the only difference being that the depth of the circular groove of the insulation cover is different, that is, the thickness of the air layer above the silicon carbide seed crystal is different.
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