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Method for preventing edge dislocation of silicon carbide crystal from slipping inwards

An edge dislocation, silicon carbide technology, applied in chemical instruments and methods, crystal growth, single crystal growth and other directions, to achieve the effect of improving crystal quality, simple operation, good repeatability and stability

Active Publication Date: 2021-11-12
SICC CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Therefore, the prior art has not been able to provide a method for producing defects in the crystal and utilizing the defects to obtain high-quality silicon carbide crystals

Method used

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  • Method for preventing edge dislocation of silicon carbide crystal from slipping inwards
  • Method for preventing edge dislocation of silicon carbide crystal from slipping inwards
  • Method for preventing edge dislocation of silicon carbide crystal from slipping inwards

Examples

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Embodiment 1

[0065] This embodiment provides a method for blocking edge dislocations and blocking edge dislocations of silicon carbide crystals from slipping inward, the method comprising the following steps:

[0066] Step 1. Place the crucible containing 1 kg of silicon carbide powder and a 4-inch silicon carbide seed crystal fixed on the crucible cover in the above-mentioned heat preservation cover, and then place the crucible together with the heat preservation cover in the growth chamber of the crystal growth furnace, that is, the structure Such as figure 1 The thermal field shown;

[0067] Step 2. Control the temperature and pressure of the crystal growth furnace and the flow of inert gas into the crystal growth furnace to clean and remove impurities in the crystal growth furnace, and then use the crystal growth furnace to grow crystals, specifically including the following stages:

[0068] Heating stage: adjust the temperature of the crystal growth furnace to 2000-2400K, and control...

Embodiment 2~8

[0073] The preparation methods of Examples 2-8 are roughly the same as those of Example 1, the only difference being that the depth of the circular groove of the insulation cover is different, that is, the thickness of the air layer above the silicon carbide seed crystal is different.

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Abstract

The invention discloses a method for preventing edge dislocation of a silicon carbide crystal from slipping inwards, which comprises the following steps that: 1, a thermal field is constructed, namely a crucible is placed in a heat preservation cover, and then the crucible and the heat preservation cover are placed in a growth cavity of a crystal growth furnace, wherein the heat preservation cover comprises a heat preservation cover, the bottom of the heat preservation cover is provided with a circular groove coaxial with a heat preservation cylinder, and the diameter of the circular groove is at least smaller than the diameter of a silicon carbide seed crystal by 1 mm and larger than or equal to two thirds of the diameter of the silicon carbide seed crystal; and 2, a silicon carbide crystal is prepared by using the thermal field, wherein an annular morphology roughly corresponding to the groove side wall position of the circular groove is formed in the position, close to the edge, of the obtained silicon carbide crystal, and the width of the annular morphology is 100-600 microns. According to the method for preventing the edge dislocation of a silicon carbide crystal from slipping inwards, a silicon carbide crystal with an annular morphology with a certain width at the edge position can be obtained, the annular morphology can prevent the edge dislocation on the outer side of the morphology from slipping towards the inner side of the annular morphology, and the crystal quality of the middle area of the silicon carbide crystal is improved.

Description

technical field [0001] The present application belongs to the technical field of silicon carbide crystal materials, and in particular relates to a method for blocking edge dislocations of silicon carbide crystals from slipping inward. Background technique [0002] Silicon carbide material (SiC) has attracted extensive attention due to its excellent semi-insulating properties, especially for high-power semiconductor devices with special requirements. SiC has become the choice of these devices due to its high temperature, high frequency, high power and other characteristics. potential material. [0003] At present, the industrial production of SiC crystals mostly adopts the physical vapor phase method (PVT method) for production, but due to its high growth conditions, it is easy to cause crystal defects during the growth process, and the formation of crystal defects limits the improvement of its performance and further development. application and development. For example, t...

Claims

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Application Information

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IPC IPC(8): C30B29/36C30B23/00
CPCC30B29/36C30B23/00
Inventor 张九阳李霞王永方赵树春张红岩高超王含冠王宁苏丽娜
Owner SICC CO LTD
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