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A kind of production process and equipment of methallyl alcohol

A technology for methallyl alcohol and production equipment, applied in the field of production technology and equipment of methallyl alcohol, can solve problems such as low mixing efficiency, insufficient utilization of methane waste, waste of energy and the like

Active Publication Date: 2022-05-13
宁波昊德化学工业股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] (1) During the production process of methallyl alcohol, it needs to be fully mixed by stirring, and the existing reactor stirring can only work on the maximum diameter range of the blade, which will make the mixing efficiency very low ;
[0004] (2) In the process of producing methallyl alcohol, the methane waste produced cannot be fully utilized, thereby causing a large amount of energy waste;
[0005] (3) During the production process of methallyl alcohol, it needs to be heated when processing methallyl alcohol, and the heated water pipe is prone to produce a large amount of scale during long-term use, so that the heating of the water pipe is affected certain influence

Method used

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  • A kind of production process and equipment of methallyl alcohol
  • A kind of production process and equipment of methallyl alcohol
  • A kind of production process and equipment of methallyl alcohol

Examples

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Embodiment 1

[0042] Such as Figure 1-Figure 10 As shown, the present embodiment discloses a production equipment for methallyl alcohol, including an oxygenation reactor 4, a first cylinder 1, a hydrogenation reactor 13 and an incinerator 20, and the oxygenation reactor 4 is provided with Stirring mechanism 23 is arranged, and described stirring mechanism 23 comprises stirring rod 2304, and the outer wall of described stirring rod 2304 is provided with several rotating blades 2302, and the upper surface of rotating blade 2302 is provided with evenly arranged scale lath 2301, and described The lower end of the stirring rod 2304 is connected with the output shaft end of the motor 30, the lower surface of the rotating vane 2302 is provided with a fixing part 2306, and the front and rear sides of the fixing part 2306 are provided with chute 2307, and the slide groove 2307 slides A sliding piece 2308 is connected, and one side of the sliding piece 2308 is provided with a branch leaf 2303 perpen...

Embodiment 2

[0052] This embodiment discloses a production process of a production equipment for methacryl alcohol, said process comprising the following steps:

[0053] S1: Put the prepared isobutylene into the oxygenation reactor 4, then connect the oxygen delivery pipe to the oxygenation nozzle 6, produce methacrolein, acetone and methacrylic acid after the reaction, and the isobutylene and oxygen are mixed in the oxygenation reactor through the above steps Fully mix in the oxygenation reactor 4, then separate methacrolein from the remaining acetone and methacrylic acid, and then conduct concentrated biochemical treatment of acetone and methacrylic acid, and the clean products produced after the treatment include carbon dioxide, water and methane , methane can be put into the incinerator 20 for utilization, while water and carbon dioxide are cleanly collected and used, so that the waste gas produced in this way can be fully utilized, and at the same time, it is more environmentally frien...

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Abstract

The invention relates to the technical field of methallyl alcohol, in particular to a production process and equipment for methallyl alcohol, including an oxygenation reactor, a first cylinder, a hydrogenation reactor and an incinerator, the oxygenation reactor There is a stirring mechanism inside, and the stirring mechanism includes a stirring rod. Several rotating blades are arranged on the outer wall of the stirring rod, and the upper surface of the rotating blade is provided with evenly arranged scale strips. The device passes through the lower surface of the rotating blade. The upper branch blade increases the ring diameter of the rotary blade to enlarge and mix the materials, and at the same time, the scale strips on the upper surface of the rotary blade can block and move the material, and then the first airtight push plate can shrink the inner cavity of the oxygenation reactor, so that The inner cavity is pressurized and fully mixed, and the incinerator is used for waste utilization through the exhaust gas methane dye. At the same time, the heat generated by the incinerator is circulated to the oxygenation reactor and hydrogenation reactor through water, and the water pipe is filtered through the filter mechanism. This way the pipes will not be clogged with scale.

Description

technical field [0001] The invention relates to the technical field of methallyl alcohol, in particular to a production process and equipment for methallyl alcohol. Background technique [0002] Methallyl alcohol, also known as "isobutenol", is an important organic intermediate used in the synthesis of perfumes, resins, etc. Use methallyl alcohol and ethylene oxide as raw materials to synthesize methallyl alcohol polyoxyethylene ether (HPEG), which is used in a new generation of high-performance concrete water reducer. Methallyl alcohol polyoxyethylene ether is easily soluble in water And a variety of organic solvents, it is an important raw material for a new generation of polycarboxylate superplasticizer. The polycarboxylate high-efficiency superplasticizer synthesized by this product has high-efficiency particle dispersion and retention capabilities, and has many advantages such as high water-reducing rate, low cement usage, good reinforcement effect, good durability, no...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J19/18C07C33/03C07C29/141B01D29/33B01D29/56
CPCB01J19/18C07C29/141C07C45/35B01D29/33B01D29/56B01J2219/00087C07C33/03C07C47/22Y02P20/10
Inventor 黄叔儒陈益斌
Owner 宁波昊德化学工业股份有限公司
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