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Preparation method and application of lotus leaf extract

A lotus leaf extract and lotus leaf technology are applied in the field of preparation of lotus leaf extract, can solve the problems of restricting the development and application of lotus leaf extract, unstable product properties, affecting the application of raw materials, etc. Product stability and the effect of promoting development and utilization

Pending Publication Date: 2021-12-14
宝萃生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In terms of liquid raw materials, I learned about a cosmetic raw material that uses 40% butanediol as a solvent and 1.5-3.5% lotus leaf extract powder to dissolve and mix. The main functional ingredient is flavonoids. This raw material has been certified by cosmos, and its Efficacy, but the raw material of the extract has a dark color, and the color will gradually become darker after the preparation of the finished cosmetic product, and the price is expensive
The current market products are prepared from the total flavonoids extracted from lotus leaves, or the flavonol glycoside macroporous resin contained in lotus leaves is processed and purified in multiple steps to prepare products; Continued darkening affects the application of raw materials; or there are many process steps, high preparation costs, and poor economic benefits. At the same time, the relationship between product efficacy and flavonoids is studied in depth, which limits the development and application of lotus leaf extract

Method used

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  • Preparation method and application of lotus leaf extract
  • Preparation method and application of lotus leaf extract
  • Preparation method and application of lotus leaf extract

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] The preparation method of a kind of lotus leaf extract as the embodiment of the present invention, comprises the following steps:

[0028] (1) Weigh 100g lotus leaf medicinal material, pulverize; reflux extraction twice with water, the water consumption is respectively 15 times, 15 times of the weight of lotus leaf medicinal material, fine filter filter, merge twice to extract filtrate, concentrate to about 100g of weight;

[0029] (2) Slowly add 5ml of hydrochloric acid solution with a mass fraction of 36% to the concentrated solution, mix well, and reflux for 5 hours.

[0030] (3) Filtrate while hot, decolorize the filtrate through alkaline anion resin, and collect the decolorized liquid.

[0031] (4) Concentrate the decolorizing solution and dry to obtain the lotus leaf extract, mix with water and butanediol, perform membrane filtration to remove impurities, and obtain the lotus leaf extract.

Embodiment 2

[0033] The preparation method of a kind of lotus leaf extract as the embodiment of the present invention, comprises the following steps:

[0034] (1) Weigh 100g lotus leaf medicinal material, pulverize; reflux extraction twice with water, the water consumption is respectively 30 times, 30 times of the weight of lotus leaf medicinal material, filter with fine filter, merge twice to extract filtrate, concentrate to about 100g of weight;

[0035] (2) Slowly add 5ml of hydrochloric acid solution with a mass fraction of 36% to the concentrated solution, mix well, and reflux for 5 hours.

[0036] (3) Filtrate while hot, decolorize the filtrate through alkaline anion resin, and collect the decolorized liquid.

[0037](4) Concentrate the decolorizing solution and dry to obtain the lotus leaf extract, mix with water and butanediol, and perform membrane removal treatment to obtain the lotus leaf extract.

Embodiment 3

[0039] The preparation method of a kind of lotus leaf extract as the embodiment of the present invention, comprises the following steps:

[0040] (1) Weigh 100g lotus leaf medicinal material, pulverize; reflux extraction twice with water, the water consumption is respectively 15 times, 15 times of the weight of lotus leaf medicinal material, fine filter filter, merge twice to extract filtrate, concentrate to about 100g of weight;

[0041] (2) Slowly add 1ml of sulfuric acid solution with a mass fraction of 98% to the concentrated solution, mix well, and reflux for 1 hour.

[0042] (3) Filtrate while hot, decolorize the filtrate through alkaline anion resin, and collect the decolorized liquid.

[0043] (4) Concentrate the decolorizing solution and dry to obtain the lotus leaf extract, mix with water and butanediol, and perform membrane removal treatment to obtain the lotus leaf extract.

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Abstract

The invention provides a preparation method and application of a lotus leaf extract. The preparation method comprises the following steps that (1), a lotus leaf medicinal material is weighed, water is added for reflux extraction according to a solid-liquid ratio of the lotus leaf medicinal material to the water of 1g to 15-30mL, extracting is carried out for 1-3 times, filtering is carried out to obtain a total flavone extracting solution, and the total flavone extracting solution is concentrated to 0.5-2 times of the weight of the lotus leaf medicinal material; (2), an acid solution is added into the concentrated solution, the adding amount of the acid solution accounts for 1%-6% of the mass of the concentrated solution, and heating reflux hydrolysis is carried out for 0.5-5 hours; (3), the hydrolysis solution is filtered while the hydrolysis solution is hot, and filtrate is decolorized to obtain a decolorized solution; and (4), the decolorized solution is dried to obtain the lotus leaf extract. According to the preparation process, an acid hydrolysis method is adopted, flavonoid substances of the lotus leaves are hydrolyzed to obtain flavonoid aglycones, and the anti-oxidation effect of the product is improved; and in addition, a decolorizing process is adopted, the decolorized product is light in color, and the color is not obviously changed in the placement process.

Description

technical field [0001] The invention belongs to the technical field of plant extraction, and in particular relates to a preparation method and application of lotus leaf extract. Background technique [0002] The distribution of lotus root in my country is very wide, and its cultivation area is between 9 million and 11 million mu. It is mainly distributed in Anhui, Hubei, Hunan, Guangxi, Guangdong, Jiangxi, Fujian, Jiangsu, Zhejiang, Shandong, Hebei and other provinces. According to the normal planting conditions Calculated, one mu of lotus root pond can produce about 300 kilograms of dried lotus leaves, and the current dried lotus leaves on the market are about 15 yuan / kg. If calculated, the lotus leaves in one mu of lotus root pond can be used reasonably , You should be able to increase your income by about 4,500 yuan a year. Nevertheless, the utilization rate of my country's lotus leaf resource is very low, less than 1% of my country's lotus leaf output. Every year, it can...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K8/9789A61Q19/00A61Q19/08
CPCA61K8/9789A61Q19/00A61Q19/08A61K2800/805
Inventor 冯磊刘逸华贺青刘露
Owner 宝萃生物科技有限公司
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