High-speed preparation method of vascular covered stent for emergency treatment of sudden coronary perforation during operation
A stent-graft and blood vessel technology, which is applied in the field of preparation of vascular stent-grafts, can solve the problems of fragility, poor stability, and easy unloading of the stent-graft, and achieves the effects of low cost and fast film formation.
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Embodiment 1
[0032] Embodiment 1: The high-speed preparation method of the vascular stent-graft for emergency treatment of sudden coronary perforation in this embodiment is carried out according to the following steps:
[0033] 1. Weigh 3g cellulose acetate, 8g isoprene, 20g crotonic acid, 1g CuI and 1.5g bipyridine;
[0034] 2. Dissolve the cellulose acetate weighed in step 1 in 20mL of N,N-dimethylformamide, heat and stir at 70°C until completely dissolved, and cool to room temperature to obtain a cellulose acetate solution;
[0035] 3. Add the isoprene weighed in step 1 to the cellulose acetate solution, and stir at room temperature for 20 hours under nitrogen protection; then fully mix the CuI and bipyridyl weighed in step 1 and add it to the cellulose acetate solution , reacted in an oil bath at 100°C for 8 hours under the protection of nitrogen, and cooled to room temperature after the reaction was completed;
[0036] 4. Add the crotonic acid weighed in step 1 to the cellulose aceta...
Embodiment 2
[0047] Embodiment 2: The high-speed preparation method of the vascular stent-graft for emergency treatment of sudden coronary perforation in this embodiment is carried out according to the following steps:
[0048] 1. Weigh 5.0g polyvinylidene fluoride, 30g acrylic acid, 1.5g CuBr and 2.0g HMTETA;
[0049] 2. Dissolve the polyvinylidene fluoride weighed in step 1 in N-methylpyrrolidone, heat and stir at 80°C until completely dissolved, and cool to room temperature to obtain a polyvinylidene fluoride solution;
[0050] 3. Add butadiene into the polyvinylidene fluoride solution, and stir for 20 hours at room temperature under the protection of nitrogen. Then fully mix the CuBr and HMTETA weighed in step 1 and add them to the polyvinylidene fluoride solution, react in an oil bath at 50°C for 8 hours under the protection of nitrogen, and cool to room temperature after the reaction is completed;
[0051] 4. Add the acrylic acid weighed in step 1 to the polyvinylidene fluoride solu...
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