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Process and device for preparing potassium ammonium polyphosphate containing chelated medium trace elements

A technology of medium and trace elements, potassium ammonium polyphosphate, applied in ammonium orthophosphate fertilizers, fertilization equipment, alkaline orthophosphate fertilizers, etc., can solve the problems of high raw material requirements and high raw material costs

Pending Publication Date: 2022-03-29
WENGFU DAZHOU CHEM CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method uses high-concentration phosphoric acid and phosphorus pentoxide, and the raw material requirements are high and the cost of raw materials is high

Method used

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  • Process and device for preparing potassium ammonium polyphosphate containing chelated medium trace elements
  • Process and device for preparing potassium ammonium polyphosphate containing chelated medium trace elements
  • Process and device for preparing potassium ammonium polyphosphate containing chelated medium trace elements

Examples

Experimental program
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Effect test

Embodiment 1

[0050] see figure 1 , the present embodiment discloses a preparation process of potassium ammonium polyphosphate containing trace elements in a chelated state, comprising the following steps:

[0051] Step 1: Add phosphoric acid, urea, potassium, and medium and trace element additives into the reactor, and stir and react at 60-90°C for 10-60 minutes to obtain a reaction slurry;

[0052] Among them, when stirring, the stirrer is made of carbon steel lined with polytetrafluoroethylene, and the jacket of the stirring equipment is kept warm. The heat source of the jacket can be steam, hot water, or heat transfer oil to improve the stirring effect;

[0053] Step 2: Add the reaction slurry obtained in step 1 into a polymerization curing device with an absolute pressure of 1-70Kpa, control the temperature of the slurry material at 140-220°C, dry and solidify the slurry into a solid material after 20-90 minutes, and control the drying and curing The polymerization rate of phosphorus ...

Embodiment 2

[0071] see Figure 1-Figure 4 , this embodiment discloses a preparation device for potassium ammonium polyphosphate containing trace elements in a chelated state, including a stirring device for stirring materials, a polymerization curing device 1 connected with the stirring device and used for solidifying the materials, and using Cooling device 2 and crushing device 3 for cooling and crushing the solidified material,

[0072] Polymerization solidifier 1 comprises cylinder body 4, is arranged in cylinder body 4 and is used for the distributor 5 that is connected with described stirring device, is arranged in cylinder body 4 and is used for the belt feeding assembly 6 of conveyor belt curing material, is arranged in belt feeding The cutter 7 at the end of the component 6, the heating component 8 arranged in the cylinder 4 and the vacuum suction component 9 communicated with the inside of the cylinder 4;

[0073] Wherein, the distributor 5 is positioned above the end of the bel...

Embodiment 3

[0085] This embodiment is further optimized on the basis of Embodiment 2. In this embodiment, there are several belt feeding assemblies 6 which are misplaced from top to bottom, and the materials on the previous belt feeding assembly 6 can fall behind. On one belt feeding assembly 6 , each belt feeding assembly 6 corresponds to a cutter 7 .

[0086] In this way, after the material is cut and scraped by the cutter 7, the material on the previous belt feeding assembly 6 can drop on the next belt feeding assembly 6, prolonging the running path of the material in the cylinder 4 and prolonging the curing and drying time. Time, improve curing and drying effect.

[0087] In a possible design, the cutting knife 7 on the lowermost belt feeding assembly 6 includes a first cutting knife 23 and a second cutting knife 24, and the first cutting knife 23 and the second cutting knife 24 are obliquely arranged on the belt feeding Above the component 6 , a material channel is formed between th...

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Abstract

The invention discloses a preparation process and device of ammonium potassium polyphosphate containing chelated medium trace elements, and the preparation process comprises the following steps: step 1, adding phosphoric acid, urea, potassium and a medium trace element additive into a reactor, and stirring to react for 10-60 minutes at 60-90 DEG C to obtain reaction slurry; step 2, adding the reaction slurry obtained in the step 1 into a polymerization curing device with the absolute pressure of 1-70Kpa, controlling the temperature of the slurry material to be 140-220 DEG C, and drying and curing the slurry into a solid material after 20-90 minutes; and 3, cooling the solid material to 30-80 DEG C, and crushing. The device is mainly used for preparing ammonium polyphosphate potassium containing chelated medium trace elements. The potassium ammonium polyphosphate prepared by the process simultaneously contains three macroelements of nitrogen, phosphorus and potassium and a plurality of medium trace elements, can comprehensively meet the requirements of different crops on nutrients, can chelate the medium trace elements, and has three macroelement nutrients of nitrogen, phosphorus and potassium, and the water solubility of the product is good.

Description

technical field [0001] The invention relates to the technical field of preparation of potassium ammonium polyphosphate, in particular to a preparation process of potassium ammonium polyphosphate containing trace elements in a chelated state; in addition, the present invention also relates to a potassium ammonium polyphosphate containing trace elements in a chelated state Prepare the device. Background technique [0002] Fertilizer is an important material in agricultural production and an important means to ensure the increase of crop yield. Under the requirement of ensuring the normal fertilizer demand of crops, how to improve the utilization efficiency of chemical fertilizers is not only related to the stable and high yield of grain, but also related to environmental protection. The general utilization rate of solid chemical fertilizer is low, the utilization rate of solid nitrogen fertilizer is between 20-50%, the utilization rate of solid phosphorus fertilizer is betwee...

Claims

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Application Information

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IPC IPC(8): C05B7/00C05G1/00
CPCC05B7/00C05D5/00C05C5/04C05D9/02C05D3/00
Inventor 刘旭陶绍程谢娟张俊刘松林付勇陈相赵强
Owner WENGFU DAZHOU CHEM CO LTD