Organic compound containing xanthone or thioxanthone structure and application thereof
An organic compound, thioxanthone technology, applied in the field of organic electroluminescent devices, can solve the problems of short-delayed luminescence lifetime, spectral instability, lag in efficiency and lifetime development, etc., achieve strong stability, improve luminous efficiency, improve effect of life
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Embodiment 14
[0063] The synthetic route of embodiment 14 compound 273
[0064]
[0065] In the three-necked flask, under the protection of nitrogen, add 0.01mol of intermediate D2, 0.012mol of 9H-xanthen-9-one, 3-(4-bromophenyl), 150mL of toluene and stir to mix, add 0.03mol Sodium tert-butoxide, 5 x 10 -5 mol of palladium acetate, heated to 120°C, and reacted for 24 hours; naturally cooled to room temperature, filtered, and the filtrate was subjected to vacuum rotary evaporation (-0.09MPa, 85°C), and passed through a neutral silica gel column to obtain compound 273, the elemental analysis structure ( Molecular formula C 49 h 30 N 2 o 2 ): theoretical value C, 86.71; H, 4.46; N, 4.13; test value: C, 86.70; H, 4.45; N, 4.14. LC-MS: The theoretical value is 678.23, and the measured value is 678.47. 1 H NMR (400MHz, Chloroform-d) δ7.96–7.90(m,5H),7.85–7.79(m,1H),7.78–7.72(m,2H),7.66(s,1H),7.65–7.59(m ,2H),7.55(dd,1H),7.50(s,1H),7.44(ddd,2H),7.41–7.33(m,9H),7.28(s,1H),7.13(d,3H),7.09...
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