Preparation method of structure color developing material with uniform color generation and low angle dependence
A low-angle, dependent technology, applied in the direction of surface coating liquid devices, coatings, special surfaces, etc., can solve the problems of uneven particle deposition, uniform color distribution, etc., to achieve uniform color rendering, improved saturation, The effect of safe and non-toxic preparation process
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Embodiment 1
[0042] Step 1: Use the improved Product D was prepared by adding 4ml tetraethyl orthosilicate into 42ml dehydrated ethanol, stirring to make it evenly mixed to make a colorless and transparent solution A; Mix 35ml of deionized water, stir to make it evenly mixed, and make a colorless and transparent solution B; mix solution A and solution B and let it stand, until the mixed solution appears milky white, then stir at 45°C at 2300 rpm The reaction was stirred at a rotating speed for 4.5 hours to obtain a uniformly mixed reaction product (milky white solution); the reaction product was cooled to room temperature, then centrifuged (centrifugation speed was 6000 rpm, centrifugation time was 20min), and the supernatant was poured off to obtain the product C: Centrifuge the product C with ethanol and deionized water respectively (centrifugation speed is 6000 rpm, centrifugation time is 20min), pour off the supernatant, repeat this process 2 times, and obtain silica precipitate prod...
Embodiment 2
[0050] Step 1: Use the improved Product D was prepared by adding 2ml of tetraethyl orthosilicate to 40ml of absolute ethanol, stirring to make it evenly mixed to make a colorless and transparent solution A; 4ml of 25%-28% ammonia, 45ml of absolute ethanol Mix 35ml of deionized water, stir to make it evenly mixed, and make a colorless and transparent solution B; mix solution A and solution B and let it stand, until the mixed solution appears milky white, then stir at 40°C at 2000 rpm The reaction was stirred at a rotating speed for 4 hours to obtain a uniformly mixed reaction product (milky white solution); the reaction product was cooled to room temperature, and then centrifuged (centrifugal speed was 8000 rpm, centrifugation time was 20min), and the supernatant was poured off to obtain product C The product C is centrifuged with ethanol and deionized water respectively (centrifugal speed is 6000 rpm, centrifugation time is 20min), pours off the supernatant, repeats this proce...
Embodiment 3
[0058] Step 1: Use the improved Product D was prepared by adding 3ml tetraethyl orthosilicate to 40ml dehydrated ethanol, stirring to make it evenly mixed to make a colorless and transparent solution A; Mix 30ml of deionized water, stir to make it evenly mixed, and make a colorless and transparent solution B; mix solution A and solution B and let it stand, until the mixed solution appears milky white, then stir at 40°C at 1800 rpm The reaction was stirred at a rotating speed for 4 hours to obtain a uniformly mixed reaction product (milky white solution); the reaction product was cooled to room temperature, and then centrifuged (centrifugal speed was 6000 rpm, centrifugation time was 20min), and the supernatant was poured off to obtain product C ; The product C is centrifuged with ethanol and deionized water respectively (centrifugal speed is 6000 rpm, centrifugation time is 20min), pours off the supernatant, repeats this process 2 times, and obtains a silica precipitate ; Dr...
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