Toughening agent with core-shell structure as well as preparation method and application of toughening agent
A technology of core-shell structure and toughening agent, which is applied in the field of core-shell structure toughening agent and its preparation, can solve the problems of reducing the mechanical properties of polydicyclopentadiene materials, achieve increased adhesion, improve impact resistance, Improve the effect of interfacial stress transfer
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Embodiment 1-5
[0035] Examples 1-5 are respectively examples of the core-shell structure toughening agent of the present invention. The preparation method of embodiment 1-5 toughening agent is: (1) heat treatment sepiolite at 250 DEG C for 4 hours, dry and also make it partly remove crystallization water at the same time, free moisture content is not higher than 0.2%; (2) Activation of sepiolite: use methanol as solvent, add sepiolite and ultrasonically stir at 55°C for 45 minutes, cool down to 45°C, add tris(2-hydroxyethyl)isocyanurate and methyl ethyl ketone peroxide to react for 2h, and dissolve the reaction solution Direct rotary steaming and drying, the obtained solid product is milled to obtain activated sepiolite particles with a particle size of 10-15 μm; (3) Preparation of the middle layer: stir the activated sepiolite particles with a small amount of styrene, and then add Cyclohexanone peroxide and hydroxyl-terminated butadiene were stirred evenly and then reacted at 140-145°C for ...
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