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Method and device for regulating and controlling structure and performance of high-entropy alloy through multi-dimensional indirect ultrasonic treatment

A high-entropy alloy and ultrasonic treatment technology, applied in metal processing equipment, casting molding equipment, casting mold components, etc., can solve the problems of horn deformation and dissolution, fast ultrasonic energy attenuation, ultrasonic equipment loss, etc., and achieve low cost , The processing process is simple, and the effect of no loss of equipment

Active Publication Date: 2022-07-29
NORTHWESTERN POLYTECHNICAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] At present, the commonly used forms and limitations of power ultrasound in the metal solidification process are: the single beam of ultrasonic waves is directly transmitted to the inside of the metal or alloy melt through the ultrasonic horn, the ultrasonic horn is in contact with the melt, and the horn It is easy to be deformed and dissolved by high temperature erosion, resulting in melt pollution and rapid loss of ultrasonic equipment. In effect, it is characterized by fast attenuation of ultrasonic energy and small range of action.

Method used

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  • Method and device for regulating and controlling structure and performance of high-entropy alloy through multi-dimensional indirect ultrasonic treatment
  • Method and device for regulating and controlling structure and performance of high-entropy alloy through multi-dimensional indirect ultrasonic treatment
  • Method and device for regulating and controlling structure and performance of high-entropy alloy through multi-dimensional indirect ultrasonic treatment

Examples

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Embodiment 1

[0076] This embodiment is a three-dimensional indirect ultrasonic treatment to refine FeNi 2 CrCuAl 0.8 The method for the microstructure and mechanical properties of high entropy alloys, the flow chart is as follows figure 1 As shown, the schematic diagram of the device used is as follows figure 2 shown.

[0077] The first step is raw material pretreatment. Use a low-speed grinder to polish off the oxide scale on the surface of the metal raw materials (Al, Cu, Fe, Ni, Cr raw materials), put it in an ultrasonic cleaner, and use alcohol to clean the oil and impurities to ensure the purity of the metal raw materials.

[0078] The second step is the filling of raw materials. The raw materials of Al, Cu, Fe, Ni and Cr with surface cleaning treatment are put into the boron nitride plug crucible in turn, and the crucible is placed in the middle of the high-frequency electromagnetic induction coil.

[0079] The third step is alloy melting. Turn on the high-frequency electromag...

Embodiment 2

[0090] The present embodiment is a method for regulating the phase content and magnetic properties of FeNiCoCuAl dual-phase high-entropy alloys by one-dimensional indirect ultrasonic treatment. The flow chart is as follows: figure 1 As shown, the schematic diagram of the device used is as follows figure 2 shown.

[0091] The first step is raw material pretreatment. Use a low-speed grinder to polish off the oxide scale on the surface of the metal raw materials (Al, Cu, Fe, Co, Ni raw materials), put it in an ultrasonic cleaner, and use alcohol to clean the oil and impurities to ensure the purity of the metal raw materials.

[0092] The second step is the filling of raw materials. The raw materials of Al, Cu, Fe, Co, and Ni with surface cleaning treatment are put into the boron nitride plug crucible in turn, and the crucible is placed in the middle of the high-frequency electromagnetic induction coil.

[0093] The third step is alloy melting. Turn on the high-frequency elec...

Embodiment 3

[0104] This embodiment is a method for regulating the phase content and magnetic properties of FeNiCoCuAl dual-phase high-entropy alloys by three-dimensional indirect ultrasonic treatment. The flow chart is as follows: figure 1 As shown, the schematic diagram of the device used is as follows figure 2 shown.

[0105] The first step is raw material pretreatment. Use a low-speed grinder to polish off the oxide scale on the surface of the metal raw materials (Al, Cu, Fe, Co, Ni raw materials), put it in an ultrasonic cleaner, and use alcohol to clean the oil and impurities to ensure the purity of the metal raw materials.

[0106] The second step is the filling of raw materials. The raw materials of Al, Cu, Fe, Co, and Ni with surface cleaning treatment are put into the boron nitride plug crucible in turn, and the crucible is placed in the middle of the high-frequency electromagnetic induction coil.

[0107] The third step is alloy melting. Turn on the high-frequency electroma...

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Abstract

The invention provides a method and device for regulating and controlling the structure and performance of a high-entropy alloy through multi-dimensional indirect ultrasonic treatment, and relates to the technical field of alloy preparation. The high-entropy alloy prepared through the method is compact in structure and free of air holes and shrinkage cavities; impurities are not introduced in the preparation process, and target alloy is not polluted; the characteristic grain size refinement degree is high, and the grain size can be refined to be 10% or below of the initial grain size; the phase content proportion can be freely regulated and controlled according to the cavitation sound pressure intensity; the ultrasonic leading-in efficiency is high, the treatment process is simple, reliable and safe, and equipment is free of loss; the treatment mode is efficient, green, energy-saving and low in cost.

Description

technical field [0001] The invention relates to the technical field of alloy preparation, in particular to a method and a device for controlling the microstructure and properties of a high-entropy alloy by multi-dimensional indirect ultrasonic treatment. Background technique [0002] High-entropy alloys are solid solution alloys composed of five or more elements with an atomic ratio of 5 to 35%. Compared with traditional metal materials, these alloys have a series of special effects, such as high-entropy effect and lattice distortion effect. , hysteresis diffusion effect and "cocktail effect", which have attracted widespread attention. In terms of element composition, high-entropy alloys are mainly divided into three systems: one is 3d transition group metal element high-entropy alloys, the other is refractory high-entropy alloys, and the third is lightweight high-entropy alloys, of which 3d transition group high-entropy alloys With Cr, Mn, Fe, Co, Ni, Cu and other commonly...

Claims

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Application Information

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IPC IPC(8): C22F3/02B22D27/20B22D27/04C22C30/02C22C1/02B22C9/06
CPCC22F3/02B22D27/20B22D27/04C22C30/02C22C1/02B22C9/061
Inventor 王建元王旭翟薇魏炳波
Owner NORTHWESTERN POLYTECHNICAL UNIV