Synthesis and preparation method of special sanitizer for underwear
A preparation method and technology of fungicides, applied in the direction of disinfectants, biocides, botanical equipment and methods, etc., can solve the problems of clothing damage, carcinogenic risk, etc., and achieve the effects of improving efficiency, transportation safety, and use safety
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Embodiment 1
[0036] Embodiment 1: the synthesis and preparation method of a kind of underwear special disinfectant mentioned in the present invention, comprise the following process:
[0037] 1) Add 15 parts of polyhexamethylene biguanide powder and 15 parts of pure water to the reaction kettle, heat up under stirring, and when the temperature is raised to 50°C, slowly add 0.5 part of phosphoric acid;
[0038] 2) Stir at a constant temperature for 0.5 hours, and add 3 parts of potassium iodide;
[0039] 3) Continue to heat up, when the temperature rises to 60°C, the constant temperature reaction is performed for 2 hours;
[0040] 4) When the reaction is completed and the temperature drops to 40°C, 61.2 parts of purified water are added;
[0041] 5) Continue stirring, add 0.2 part of disodium EDTA, 0.1 part of orange essence, and 5 parts of coco acid diethanolamide in sequence, and stir well;
[0042] 6) Adjust pH to 6.8 with 0.5 part of sodium hydroxide;
[0043] 7) The obtained solutio...
Embodiment 2
[0044] Embodiment 2: the synthesis and preparation method of a kind of special sterilizing agent for underwear mentioned in the present invention, comprise the following process:
[0045] 1) Add 20 parts of polyhexamethylene biguanide powder and 20 parts of pure water to the reaction kettle, heat up under stirring, and slowly add 1 part of phosphoric acid when the temperature rises to 50°C;
[0046] 2) Stir at constant temperature for 1 hour, and add 4 parts of potassium iodide;
[0047] 3) Continue to heat up, when the temperature rises to 70°C, the constant temperature reaction is performed for 3 hours;
[0048] 4) After the reaction is completed, when the temperature drops to 40°C, add 47.5 parts of pure water;
[0049] 5) Continue stirring, add 0.3 parts of disodium EDTA, 0.2 parts of wormwood essence, and 6 parts of coco acid diethanolamide in sequence, and stir well;
[0050] 6) Adjust the pH to 7.5 with 1 part of sodium hydroxide;
[0051] 7) The obtained solution is...
Embodiment 3
[0052] Embodiment 3: the synthesis and compound method of a kind of special-purpose sterilizing agent for underwear mentioned in the present invention, comprise the following process:
[0053] 1) Add 25 parts of polyhexamethylene biguanide powder and 25 parts of pure water to the reaction kettle, heat up under stirring, and slowly add 1.5 parts of phosphoric acid when the temperature rises to 50°C;
[0054] 2) Stir at a constant temperature for 1 hour, and add 5 parts of potassium iodide;
[0055] 3) Continue to heat up, when the temperature rises to 70°C, the constant temperature reaction is performed for 4 hours;
[0056] 4) After the reaction is completed, when the temperature drops to 40°C, add 32.7 parts of pure water;
[0057] 5) Continue stirring, add 0.5 part of disodium EDTA, 0.3 part of pine essence, and 8 parts of coco acid diethanolamide in sequence, and stir well;
[0058] 6) Adjust pH to 8.0 with 2 parts of sodium hydroxide;
[0059] 7) The obtained solution i...
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