Processing technology of low-static glass fiber chopped strands with good bundling property
A technology of glass fiber and processing technology, which is applied in the field of processing technology of finely bundled and low-static glass fiber chopped strands. It can solve the problems of low bundleability and difficult dispersion of finishing agents, and achieve the effect of enhancing dispersion
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Embodiment 1
[0052] This embodiment is the processing technology of the good bundled low-static glass fiber chopped strands, and the good bundled low-static glass fiber chopped strands are prepared by the following steps:
[0053] S1: Use sizing agent and silane coupling agent to pretreat glass fiber strands, and then use a cutting device to cut into short filaments;
[0054] S2: Use finishing agent to spray the cut filaments;
[0055] S3: performing stuffing and wake-up treatments in sequence, and finally sealing and packaging to obtain the good bundled low-static glass fiber chopped strands;
[0056] The finishing agent includes the following components in parts by weight:
[0057] 0.5 part of coupling agent, 2 parts of emulsifier, 2 parts of antistatic agent, 0.1 part of softener, 95.4 parts of non-ionic water;
[0058] The emulsifier is prepared by the following steps:
[0059] S11: adopt a vacuum distillation device, 4-hexylphenol is distilled, and the colorless transparent fractio...
Embodiment 2
[0072] The difference between this embodiment and Embodiment 1 is:
[0073] The finishing agent includes the following components in parts by weight:
[0074] 0.4 part of coupling agent, 1 part of emulsifier, 1 part of antistatic agent, 0.6 part of softener, and 97 parts of non-ionic water;
[0075] The emulsifier is prepared by the following steps:
[0076] S11: adopt a vacuum distillation device, 4-hexylphenol is distilled, and the colorless transparent fraction distilled is collected for subsequent use;
[0077] S12: put 20g of Na 2 SO 3 and 13g of NaHSO 3 Dissolved in distilled water and placed in a reaction four-necked flask equipped with an electric stirring device, a thermometer and a condensing device, at a temperature of 40 ° C, add 9 g of epichlorohydrin dropwise, and control the rate of addition to be 2 drops / s. After the addition, it was cooled with an ice-water bath and continued to react for 4 h, filtered under reduced pressure, and dried in vacuo to obtain ...
Embodiment 3
[0089] The difference between this embodiment and Embodiment 1 is:
[0090]The finishing agent includes the following components in parts by weight:
[0091] 0.2 part of coupling agent, 1.5 part of emulsifier, 1 part of antistatic agent, 0.4 part of softener, 96.9 parts of non-ionic water;
[0092] The emulsifier is prepared by the following steps:
[0093] S11: adopt a vacuum distillation device, 4-hexylphenol is distilled, and the colorless transparent fraction distilled is collected for subsequent use;
[0094] S12: put 20g of Na 2 SO 3 and 13g of NaHSO 3 Dissolved in distilled water and placed in a reaction four-necked flask equipped with an electric stirring device, a thermometer and a condensing device, at a temperature of 30 ° C, add 9 g of epichlorohydrin dropwise, and control the rate of addition to be 1 drop / s. After the addition, it was cooled with an ice-water bath and continued to react for 4 h, filtered under reduced pressure, and dried in vacuo to obtain In...
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