Lubricant for plastic working of metal material
A technology of plastic processing and metal materials, applied in the direction of lubricating compositions, base materials, petroleum industry, etc., can solve the problems that can not be widely used to replace chemical, can not obtain lubricants, etc.
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Embodiment 1~3
[0049] Examples 1-3, Comparative Examples 1-2
[0050] The lubricant composition was prepared in the ratio shown in Table 1. After dissolving the water-soluble inorganic salt in water, the phenol resin is dissolved and stirred well to prepare it. After dipping a Bowden friction test piece (material: SPC steel plate, 150 mm×75 mm×1.0 mm) in this lubricant composition for 30 seconds, it was dried at 100° C. for 30 minutes. Then, calcium stearate powder (manufactured by NOF Co., Ltd.) was evenly sprinkled on the entire dried film, and then it was used for the Bowden friction test.
[0051] In addition, before applying the lubricant composition for the Boden friction test, the test piece was subjected to the following pretreatment steps (1) to (2) and dried with hot air.
[0052] (1) Alkali degreasing (manufactured by Japan Parkerlizing Co., Ltd., fine lotion 4360, concentration 20 g / l, temperature 60° C., immersion for 10 minutes).
[0053] (2) Washing with water Spray washing...
Embodiment 4~17
[0055] Embodiment 4~17, comparative example 3~6
[0056] Modulate the lubricant composition according to the ratio shown in Table 2. After dissolving the water-soluble inorganic salt in water, the urethane resin, polyvinyl alcohol, phenol resin or acrylate resin is dissolved and fully stirred. Additive 1 (lubricant) shown in Table 2 (polyethylene wax dispersion, calcium stearate dispersion, polytetrafluoroethylene or palm oil emulsion) was added and stirred to prepare a lubricant composition. After immersing the Bowden friction test piece (material: SPC steel plate, 150mm×75mm×1.0mm) in this lubricant composition for 30 seconds, it was dried at 100° C. for 30 minutes, and used for the Bowden friction test. The Bowden friction test and the pretreatment of the Bowden test pieces were carried out in the same manner as in Examples 1-3.
[0057] After immersing the rear punched test piece in the lubricant composition for 30 seconds, place it in an oven at 100° C. for 30 minutes, ...
Embodiment 18~34
[0074] The lubricant composition was prepared in the ratio shown in Table 3. That is, after carrying out the same operation according to Examples 4-10, add additive B (molybdenum disulfide, graphite, boron nitride, graphite fluoride, vulcanized vegetable oil, MoDTC, MoDTP, ZnDTP or phosphite) with 2% by weight of the surface The active agent (non-ionic) is added after pre-mixing with water.
[0075] Coating treatment, Bowden friction test and rear punching test were performed in the same manner as in Examples 4-10.
[0076] The above test results are shown in Tables 1 to 3. As can be seen from Tables 1 to 3, Examples 1 to 34 using the lubricant composition for plastic working of metal materials according to the present invention exhibited excellent lubricity with simple operations. On the other hand, Comparative Examples 1 to 6, which were outside the scope of the present invention and could not satisfy the constitutional conditions of the present invention, failed to satisf...
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