Hardness-improved oxidation-resistant material as well as preparation method and application thereof
A technology of oxidation resistance and hardness, applied in the field of materials, it can solve the problems of low hardness and insufficiency of oxidation.
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[0048] Still another embodiment of the present invention provides a method for preparing a hardness-improved oxidation-resistant material. The preparation method comprises the following steps: by mass percentage, prepare materials according to 30%-60% of boron nitride, 35%-60% of mica, 0-20% of thermal conductive agent and 0-10% of glass-ceramic; Mica, thermally conductive agent and glass-ceramic blend. The preparation method is simple and feasible, and is suitable for industrial production.
[0049] In a specific example, after the boron nitride, mica, thermal conductive agent and glass-ceramic are mixed, the following step is further included: mixing the mixed material with an anti-settling agent, a water reducing agent, a dispersing agent and a defoaming agent; Among them, in terms of the mass percentage of the sum of the mass of boron nitride, mica, thermal conductive agent and glass-ceramic, the mass percentage of anti-settling agent is 0.5% to 2%, and the mass percentag...
Embodiment 1
[0062] The preparation method of the hardness-improved oxidation-resistant material in this embodiment includes the following steps:
[0063] S101: In terms of mass percentage, prepare and mix materials according to 50% of hexagonal boron nitride, 40% of mica, 5% of silicon carbide and 5% of glass-ceramic to obtain a mixture.
[0064] S102: Add 50% of the ethanol by mass of the mixture to the mixture obtained in S101, and perform ball milling for 5 hours. After ball milling, it was dried, and then passed through a 200-mesh sieve to obtain powder.
[0065] S103: adding polyamide wax, ceramic water reducing agent and deionized water to the powder obtained in S102 and stirring evenly, then adding a modified silicone defoamer and continuing to stir to obtain a slurry. Among them, in terms of the mass percentage of the sum of the mass of hexagonal boron nitride, mica, silicon carbide and glass-ceramic, the mass percentage of anti-settling agent is 0.8%, the mass percentage of cera...
Embodiment 2
[0069] Compared with Example 1, the difference of this example is that, in terms of mass percentage, the materials are prepared according to 30% of hexagonal boron nitride, 60% of mica, 5% of silicon carbide and 5% of glass-ceramic.
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