Flavored oil and preparation method thereof
A technology for flavor oils and flavor substances, which is applied in the production/processing of edible oil/fat, edible oil/fat, food science, etc. Low cost, better oil flavor
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[0019] The invention provides a preparation method of flavor oil, the preparation method comprises the following steps, or is composed of the following steps:
[0020] (1) Preparation of oilseed meal;
[0021] (2) acid hydrolysis: the oilseed meal is mixed with acid to carry out acid hydrolysis to obtain hydrolyzate;
[0022] (3) Maillard reaction: in the hydrolyzate, add reducing sugar, or amino acid, or their combination, and continuously stir to carry out Maillard reaction after mixing;
[0023] (4) Extraction of flavor substances: after the Maillard reaction is completed, basic vegetable oils and fats are added, heated and stirred to extract flavor substances, and the supernatant liquid is separated after centrifugation to obtain flavor oils and fats.
[0024] In the present invention, the oil and fat are preferably vegetable fats and oils. "Flavoured oil and fat" refers to vegetable oils and fats which are further improved and enhanced in flavor on the basis of vegetabl...
Embodiment 1
[0043] Select rapeseed, clean up and remove impurities, add 10wt% water, fry the seeds at 160°C for 30min, after pressing, degreasing with 150mL n-hexane to obtain rapeseed meal (water content is 1.18g / 100g meal, fat content is 7.4g / 100g meal). Weigh 15 g of crushed rapeseed meal into a beaker, add 75 mL of hydrochloric acid (mass concentration 5%), place it in a magnetic stirrer to fully mix and preheat, and then place it in a 105°C oven for hydrolysis for 16 hours. The hydrolyzed solution was adjusted to pH=4, 0.5 g of xylose was added, heated and stirred, poured into a high-temperature and high-pressure reaction kettle, and reacted at 160° C. for 3 hours. After the reaction, 45 g of first-grade rapeseed oil was added, stirred at 200 r / min, and extracted at 90° C. for 1 h. The upper layer of oil was transferred to a 50mL centrifuge tube and centrifuged at 5000r / min for 10min. Transfer the upper clarified oil to a sealed bottle, which is the flavored rapeseed oil sample, an...
Embodiment 2
[0051] Select sunflower seeds, clean and remove impurities, add 6wt% of water, fry the seeds for 30min at a temperature of 130°C, and after pressing, degreasing with 150mL of n-hexane to obtain sunflower seed meal (water content is 1.25g, 100g meal, fat content is 5.6g / 100g meal). Weigh 20 g of crushed sunflower seed meal into a beaker, add 150 mL of hydrochloric acid (6%), place it in a magnetic stirrer to fully mix and preheat, and then place it in a 90°C water bath for hydrolysis for 12 hours. The acid hydrolyzed solution was adjusted to pH=6, 0.5 g of glutamic acid, 0.5 g of lysine, and 0.25 g of xylose were added, heated and stirred, poured into a high-temperature and high-pressure reaction kettle, and reacted at 170° C. for 2 hours. After the reaction, 80 g of first-class sunflower oil was added, stirred at 200 r / min, and extracted at 90° C. for 20 min. The upper layer of oil was transferred to a 50mL centrifuge tube and centrifuged at 5000r / min for 10min. Transfer the...
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