Bamboo viscose fibre and its preparing method
A viscose fiber and bamboo technology, applied in the field of fiber production, can solve the problems of uncomfortable wearing, inability to achieve antibacterial, loss and other problems
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Embodiment 1
[0032] (1) Pretreatment: liquid ratio 1:2.5, temperature 160°C, time 180 minutes.
[0033] (2) Cooking: the amount of alkali used is 8% of the absolute dry pulp in terms of NaOH, the liquid ratio is 1:4, the hydrogen peroxide is 1% of the absolute dry pulp, the oxygen pressure is 0.70Mpa, the total heating time is 150 minutes, and the holding temperature is 125°C , holding time 11 hours.
[0034] (3) Chlorination: the amount of chlorine used for chlorination is 1% of absolute dry pulp, the concentration of chlorinated pulp is 3.2%, the chlorination time is 60 minutes, and the chlorination temperature is normal temperature.
[0035] (4) Alkali refining: pulp concentration 5%, NaOH consumption 2% to absolute dry pulp, refining temperature 90°C, hydrogen peroxide to 0.5% absolute dry pulp, oxygen flow to 0.4% absolute dry pulp, time 100 minutes.
[0036] (5) Bleaching:
[0037] The pH of the first stage is 9, the amount of chlorine used is 1% to the amount of absolute dry pulp,...
Embodiment 2
[0062] (1) Pretreatment: liquid ratio 1:3, temperature 170°C, time 150 minutes.
[0063] (2) Cooking: the amount of alkali used is 13% of the absolute dry pulp in terms of NaOH, the liquid ratio is 1:5, the hydrogen peroxide is 2% of the absolute dry pulp, the oxygen pressure is 0.80Mpa, the total heating time is 200 minutes, and the holding temperature is 128°C , holding time 8.5 hours.
[0064] (3) Chlorination: the amount of chlorine used for chlorination is 2.5% to the absolute dry pulp amount, the chlorination pulp is thick 3.0%, the chlorination time is 50 minutes, and the chlorination temperature is normal temperature.
[0065] (4) Alkali refining: pulp concentration 8%, NaOH consumption 4% to absolute dry pulp, refining temperature 80°C, hydrogen peroxide 1% to absolute dry pulp, oxygen flow rate 0.5% to absolute dry pulp, time 80 minutes.
[0066] (5) Bleaching:
[0067] The pH of the first stage is 10, the amount of chlorine used is 2% to the amount of absolute dry...
Embodiment 3
[0092] (1) Pretreatment: liquid ratio 1:3.5, temperature 180°C, time 100 minutes.
[0093] (2) Cooking: the amount of alkali used is 16% of the absolute dry pulp in terms of NaOH, the liquid ratio is 1:6, the hydrogen peroxide is 3% of the absolute dry pulp, the oxygen pressure is 0.90Mpa, the total heating time is 240 minutes, and the holding temperature is 132°C , holding time 6 hours.
[0094] (3) Chlorination: the amount of chlorine used for chlorination is 4% to the absolute dry pulp amount, the thick 2.8% of the chlorinated pulp, the chlorination time is 40 minutes, and the chlorination temperature is normal temperature.
[0095] (4) Alkali refining: pulp concentration 10%, NaOH consumption 6% relative to absolute dry pulp, refining temperature 70°C, hydrogen peroxide relative to absolute dry pulp 1.5%, oxygen flow rate relative to absolute dry pulp 0.6%, time 60 minutes.
[0096] (5) Bleaching:
[0097] The pH of the first stage is 11, the amount of chlorine used is 3...
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