Method for baking industrial iron base catalyzer through Fischer-Tropsch synthesis from plasma phase
An iron-based catalyst and Fischer-Tropsch synthesis technology, which is applied in chemical instruments and methods, catalyst activation/preparation, physical/chemical process catalysts, etc., can solve the problems such as the wear and tear of the catalyst CO conversion rate activity data, and achieve superiority Reactive properties, improved wear resistance, and low damage rate
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Embodiment 1
[0026] Spherical industrial Fe / Cu / K / SiO prepared by combining continuous coprecipitation and spray drying 2 Catalyst is laid flat on the material conveyor belt of the 10m long three-stage swirling airflow belt dryer with a conveying hopper, and the thickness of the catalyst is adjusted to 40 mm with the flashboard on the material conveyor belt. Adjust the hot air inlet temperature in the heating section of the belt dryer to 200°C, the hot air temperature in the constant temperature section of the roasting section to 380°C, and the exhaust air outlet temperature in the cooling section to 120°C. Adjust the transmission speed of the three-stage material conveyor belt to 0.2 m / h, 0.8 m / h and 0.25 m / h respectively, and the residence time of the catalyst in the heating section of the belt dryer, the roasting constant temperature section and the cooling section are respectively 10 hours, 7.5 hours and 8 hours. After the catalyst passes through the cooling section, it is separated fr...
Embodiment 2
[0028] According to embodiment 1 step Fe / Mn / K / SiO 2 The thickness of the catalyst on the material conveyor belt is adjusted to 50mm. Adjust the hot air inlet temperature in the heating section of the belt dryer to 220°C, the hot air temperature in the constant temperature section of the roasting to 400°C, and the exhaust air outlet temperature in the cooling section to 120°C. Adjust the transmission speed of the three-stage material conveyor belt to 0.2 m / h, 1.0 m / h and 0.4 m / h respectively, and the residence time of the catalyst in the heating section of the belt dryer, the roasting constant temperature section and the cooling section are respectively 10 hours, 6 hours and 5 hours. After the catalyst passes through the cooling section, it is separated from the material conveyor belt of the dryer, and the fresh catalyst that has been roasted and directly used for industrial slurry phase Fischer-Tropsch synthesis is obtained. The main structural and performance indicators of ...
Embodiment 3
[0030] According to embodiment 1 step Fe / Cu / La / K / SiO 2 The thickness of the catalyst on the material conveyor belt is adjusted to 60mm. Adjust the hot air inlet temperature in the heating section of the belt dryer to 250°C, the hot air temperature in the constant temperature section of the roasting section to 450°C, and the exhaust air outlet temperature in the cooling section to 160°C. Adjust the transmission speed of the three-stage material conveyor belt to 0.2 m / h, 1.0 m / h and 0.4 m / h respectively, and the residence time of the catalyst in the heating section of the belt dryer, the roasting constant temperature section and the cooling section are respectively 10 hours, 6 hours and 5 hours. After the catalyst passes through the cooling section, it is separated from the material conveyor belt of the dryer, and the fresh catalyst that has been roasted and directly used for industrial slurry phase Fischer-Tropsch synthesis is obtained. The main structural and performance ind...
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